A powder mill was a
mill
Mill may refer to:
Science and technology
*
* Mill (grinding)
* Milling (machining)
* Millwork
* Textile manufacturing, Textile mill
* Steel mill, a factory for the manufacture of steel
* List of types of mill
* Mill, the arithmetic unit of the A ...
where
gunpowder
Gunpowder, also commonly known as black powder to distinguish it from modern smokeless powder, is the earliest known chemical explosive. It consists of a mixture of sulfur, carbon (in the form of charcoal) and potassium nitrate ( saltpeter) ...
is made from
sulfur
Sulfur (or sulphur in British English) is a chemical element with the symbol S and atomic number 16. It is abundant, multivalent and nonmetallic. Under normal conditions, sulfur atoms form cyclic octatomic molecules with a chemical formul ...
,
saltpeter
Potassium nitrate is a chemical compound with the chemical formula . This alkali metal nitrate salt is also known as Indian saltpetre (large deposits of which were historically mined in India). It is an ionic salt of potassium ions K+ and nit ...
and
charcoal.
Milling steps
Crude grinding and mixing operations such as the
Frankford Powder-Mill of
Philadelphia
Philadelphia, often called Philly, is the largest city in the Commonwealth of Pennsylvania, the sixth-largest city in the U.S., the second-largest city in both the Northeast megalopolis and Mid-Atlantic regions after New York City. Sinc ...
were a
cottage industry until the
industrial revolution
The Industrial Revolution was the transition to new manufacturing processes in Great Britain, continental Europe, and the United States, that occurred during the period from around 1760 to about 1820–1840. This transition included going f ...
brought improved product quality through the following procedures:
*
Charcoal was often manufactured nearby from locally available trees, but the heating retorts were typically separated from the other buildings to minimize fire danger. Trees with low value as sources of
lumber
Lumber is wood that has been processed into dimensional lumber, including beams and planks or boards, a stage in the process of wood production. Lumber is mainly used for construction framing, as well as finishing (floors, wall panels, w ...
were debarked, dried, and cut to uniform length to fit into iron retorts with
cast iron
Cast iron is a class of iron– carbon alloys with a carbon content more than 2%. Its usefulness derives from its relatively low melting temperature. The alloy constituents affect its color when fractured: white cast iron has carbide impu ...
doors. The
retorts were carefully packed to leave as little air space as possible, and the retort doors were closed and sealed with clay to prevent entry of air as the retorts were heated by external fires. Volatile gas generated by the heating process was vented through a small
flue
A flue is a duct, pipe, or opening in a chimney for conveying exhaust gases from a fireplace, furnace, water heater, boiler, or generator to the outdoors. Historically the term flue meant the chimney itself. In the United States, they are ...
at the top of each retort. After the external fires were extinguished, the retorts were allowed to cool before the doors were opened to remove the charcoal.
* High purity
sulfur
Sulfur (or sulphur in British English) is a chemical element with the symbol S and atomic number 16. It is abundant, multivalent and nonmetallic. Under normal conditions, sulfur atoms form cyclic octatomic molecules with a chemical formul ...
usually required little preparation other than grinding to a powder. Separate grinding mills reduced cool charcoal and sulfur to fine powders.
[
* Crude ]saltpeter
Potassium nitrate is a chemical compound with the chemical formula . This alkali metal nitrate salt is also known as Indian saltpetre (large deposits of which were historically mined in India). It is an ionic salt of potassium ions K+ and nit ...
(KNO3) was dissolved in a pot of boiling water. After boiling, a small amount of floating glue might be added to the hot water to aid skimming off floating impurities. The hot solution was then carefully decanted to avoid suspending insoluble
In chemistry, solubility is the ability of a substance, the solute, to form a solution with another substance, the solvent. Insolubility is the opposite property, the inability of the solute to form such a solution.
The extent of the solub ...
solid impurities settled to the bottom of the pot. The hot decanted liquid was distributed into shallow wooden vats where evaporative cooling would remove excess water. Purified potassium nitrate
Potassium nitrate is a chemical compound with the chemical formula . This alkali metal nitrate salt is also known as Indian saltpetre (large deposits of which were historically mined in India). It is an ionic salt of potassium ions K+ and ni ...
recrystallized while the cooling solution was gently agitated with broad hoes to prevent formation of large crystal
A crystal or crystalline solid is a solid material whose constituents (such as atoms, molecules, or ions) are arranged in a highly ordered microscopic structure, forming a crystal lattice that extends in all directions. In addition, macr ...
s.[
* Powdered sulfur and charcoal were combined in appropriate ratios with moist saltpeter crystals, and the moist paste was mixed and compacted by kneading beneath heavy rotating wheels in a press mill.][
* The compressed cake was transferred to a corning mill or kernelling mill to be cut into pieces of approximately correct size by bronze- or ]zinc
Zinc is a chemical element with the symbol Zn and atomic number 30. Zinc is a slightly brittle metal at room temperature and has a shiny-greyish appearance when oxidation is removed. It is the first element in group 12 (IIB) of the periodic t ...
-toothed wheels.[
* Kernelling mill products were sorted by size using leather ]sieve
A sieve, fine mesh strainer, or sift, is a device for separation process, separating wanted elements from unwanted material or for controlling the particle size distribution of a sample, using a screen such as a warp and weft, woven mesh or n ...
s. Oversize product was returned to the kernelling mill, while undersize product was returned to the press mill.[
* Sorted kernels of desired size were dried and mixed with ]graphite
Graphite () is a crystalline form of the element carbon. It consists of stacked layers of graphene. Graphite occurs naturally and is the most stable form of carbon under standard conditions. Synthetic and natural graphite are consumed on la ...
to be tumbled in glazing mill barrels. Graphite coating reduced the tendency of grains to stick together in storage.[
* Glazed product was typically packaged in wooden kegs. Filled kegs were transported away from the mill as soon as possible to a ]powder magazine Powder Magazine, Powder House, or Powderworks may refer to:
*Powder tower or powder house, a building used to store gunpowder or explosives; common until the 20th century
*Gunpowder magazine, a building designed to store gunpowder in wooden barrels ...
for wholesale distribution. The potential for destructive energy release from powder magazine accidents required the magazines to be distant from both the powder mill and other places of business or habitation.[
]
Explosions
Gunpowder is very easily ignited by static electricity
Static electricity is an imbalance of electric charges within or on the surface of a material or between materials. The charge remains until it is able to move away by means of an electric current or electrical discharge. Static electricity is n ...
or lightning strike
A lightning strike or lightning bolt is an electric discharge between the atmosphere and the ground. Most originate in a cumulonimbus cloud and terminate on the ground, called cloud-to-ground (CG) lightning. A less common type of strike, groun ...
s, and most powder mills experienced occasional accidental explosion
An explosion is a rapid expansion in volume associated with an extreme outward release of energy, usually with the generation of high temperatures and release of high-pressure gases. Supersonic explosions created by high explosives are kno ...
s. Powder mill explosions typically destroyed an entire building and killed those working in the vicinity of the building. Explosions might throw flaming debris which could ignite other buildings. Successful mills were typically built as an arrangement of separate buildings to minimize the loss from any single building explosion. Buildings were separated by enough distance to minimize the risk of being damaged by an explosion in an adjacent building. Buildings were usually built of stone with one weak wooden wall and roof to direct the force and debris from an accidental explosion toward a river or an open field.[
]
Power supply
Powder mills were originally powered by windmill
A windmill is a structure that converts wind power into rotational energy using vanes called sails or blades, specifically to mill grain (gristmills), but the term is also extended to windpumps, wind turbines, and other applications, in so ...
s, water mill
A watermill or water mill is a mill that uses hydropower. It is a structure that uses a water wheel or water turbine to drive a mechanical process such as milling (grinding), rolling, or hammering. Such processes are needed in the productio ...
s or horse mills. Despite later availability of steam engine
A steam engine is a heat engine that performs mechanical work using steam as its working fluid. The steam engine uses the force produced by steam pressure to push a piston back and forth inside a cylinder. This pushing force can be ...
s, the older power sources did not require a fire to generate steam
Steam is a substance containing water in the gas phase, and sometimes also an aerosol of liquid water droplets, or air. This may occur due to evaporation or due to boiling, where heat is applied until water reaches the enthalpy of vaporizat ...
, and avoided the possibility of sparks which might ignite the gunpowder. Some 20th-century powder mills used electric power. Before the availability of safe electrical power, some of the most successful mills were built along rivers where water could be distributed through a power canal
A Power canal refers to a canal used for hydraulic power generation, rather than for transport of watercraft. The power canal was a major factor in the Industrial revolution in New England in the 19th century. Most early power canals were mill ...
to individual buildings and intermediate products could be floated from one building to the next. The power canal offered a supply of firefighting water, and the adjacent river was a relatively safe direction to focus explosion debris. Where water transport was impractical, intermediate products were often transported in wagons pulled by draft animal
A working animal is an animal, usually domesticated, that is kept by humans and trained to perform tasks instead of being slaughtered to harvest animal products. Some are used for their physical strength (e.g. oxen and draft horses) or fo ...
s. The wagons were often built entirely of wood held together with wooden pegs, and draft animals were usually unshod to avoid sparks from steel shoes or nails.[
]
In the United States
The 1810 census reported 208 powder mills in the United States.[ In 1802, the DuPont family started their industrial enterprises in the ]United States
The United States of America (U.S.A. or USA), commonly known as the United States (U.S. or US) or America, is a country primarily located in North America. It consists of 50 U.S. state, states, a Washington, D.C., federal district, five ma ...
by building the Eleutherian Mills
From 1802 to 1921, Eleutherian Mills was a gunpowder mill site used for the manufacture of explosives founded by Eleuthère Irénée du Pont, which grew into the DuPont company. The name also refers to the house on the hill above the mills, whi ...
on the Brandywine Creek in Delaware
Delaware ( ) is a state in the Mid-Atlantic region of the United States, bordering Maryland to its south and west; Pennsylvania to its north; and New Jersey and the Atlantic Ocean to its east. The state takes its name from the adjacen ...
. Four mills were manufacturing 69 percent of United States gunpowder when gunpowder production peaked during the American Civil War
The American Civil War (April 12, 1861 – May 26, 1865; also known by other names) was a civil war in the United States. It was fought between the Union ("the North") and the Confederacy ("the South"), the latter formed by state ...
. They were the DuPont mill, the Hazard Powder Company of Hazardville, Connecticut, the Oriental Powder Company of Windham, Maine, and the Laflin Powder Company of Newburgh, New York
Newburgh is a city in the U.S. state of New York, within Orange County. With a population of 28,856 as of the 2020 census, it is a principal city of the Poughkeepsie–Newburgh–Middletown metropolitan area. Located north of New York City, ...
. The Confederate Powderworks
The Confederate Powderworks (a.k.a. the Augusta Powderworks) was a gunpowder factory during the American Civil War, the only permanent structures completed by the Confederate States of America.Bragg, C. L. (2001) "The Augusta powder works: The Con ...
of Augusta, Georgia
Augusta ( ), officially Augusta–Richmond County, is a consolidated city-county on the central eastern border of the U.S. state of Georgia. The city lies across the Savannah River from South Carolina at the head of its navigable portion. Georg ...
produced 6,000 tonnes of gunpowder from 1862 to 1865, but was dismantled after the war. The Laflin company merged into the Laflin & Rand Powder Company after the war, and with the other three large northern mills formed the United States Gunpowder Trade Association in 1872 including the American Powder Mills of Maynard, Massachusetts
Maynard is a town in Middlesex County, Massachusetts, United States. The town is located 22 miles west of Boston, in the MetroWest and Greater Boston region of Massachusetts and borders Acton, Concord, Stow and Sudbury. The town's populatio ...
, the Austin Powder Company
Austin Cartridge Company was an Austin Powder Company subsidiary manufacturing cartridge ammunition for small arms. The company made shotgun shells and rimfire cartridges from 1895 until purchased by Western Cartridge Company in 1907.
History
A ...
of Glenwillow, Ohio
Glenwillow is a village in Cuyahoga County, Ohio, United States. The population was 923 at the 2010 census.
History
The Village of Glenwillow was carved out of Solon Township and established in 1893 as a company town by Austin Powder Company. ...
, and the Miami Powder Company of Goes Station, Ohio. Most smaller mills were unable to compete with this trade association, popularly known as the powder trust; although regionally important mills including the California Powder Works of Santa Cruz, California
Santa Cruz ( Spanish for "Holy Cross") is the county seat and largest city of Santa Cruz County, in Northern California. As of the 2020 census, the city population was 62,956. Situated on the northern edge of Monterey Bay, Santa Cruz is a pop ...
, the Equitable Powder Company of East Alton, Illinois, and the Great Western Powder Works of Kings Mills, Ohio
Kings Mills is a census-designated place in the southwestern corner of Deerfield Township, Warren County, Ohio, United States, on the western shore of the Little Miami River. Located along I-71 twenty miles northeast of Cincinnati, it is less t ...
successfully transitioned to manufacture of smokeless powder
Finnish smokeless powderSmokeless powder is a type of propellant used in firearms and artillery that produces less smoke and less fouling when fired compared to gunpowder ("black powder"). The combustion products are mainly gaseous, compared to ...
cartridges. As smokeless powder and high explosive
An explosive (or explosive material) is a reactive substance that contains a great amount of potential energy that can produce an explosion if released suddenly, usually accompanied by the production of light, heat, sound, and pressure. An e ...
s replaced gunpowder for most purposes, DuPont became the major manufacturer of United States gunpowder until discontinuing production in 1971. Subsequent production for use in pyrotechnics
Pyrotechnics is the science and craft of creating such things as fireworks, safety matches, oxygen candles, Pyrotechnic fastener, explosive bolts and other fasteners, parts of automotive airbags, as well as gas-pressure blasting in mining, quarry ...
and antique firearms has been undertaken by smaller firms whose operations are often ended by the persistent hazard of accidental explosions.
Europe
Notable European mills include:
* Ballincollig Royal Gunpowder Mills, Cork, Ireland
Ireland ( ; ga, Éire ; Ulster Scots dialect, Ulster-Scots: ) is an island in the Atlantic Ocean, North Atlantic Ocean, in Northwestern Europe, north-western Europe. It is separated from Great Britain to its east by the North Channel (Grea ...
* Faversham explosives industry, Faversham
Faversham is a market town in Kent, England, from London and from Canterbury, next to the Swale, a strip of sea separating mainland Kent from the Isle of Sheppey in the Thames Estuary. It is close to the A2 road (Great Britain), A2, which foll ...
, England
* Grenelle Mill - France
* Poudrerie nationale de Vonges, Vonges, Côte-d'Or, France
* Waltham Abbey Royal Gunpowder Mills, Waltham Abbey, Essex, England
References
{{Authority control
Firearm industry
Grinding mills