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Titanium Powder
Titanium powder metallurgy (P/M) offers the possibility of creating net shape or near net shape parts without the material loss and cost associated with having to machine intricate components from wrought billet. Powders can be produced by the blended elemental technique or by pre-alloying and then consolidated by metal injection moulding, hot isostatic pressing, direct powder rolling or laser engineered net shaping. Titanium powder is used in aerospace, medical implants, 3D printing, powder metallurgy, and surface coatings due to its strength, low weight, and corrosion resistance. It also plays a vital role in energy generation, sports equipment, and as a catalyst in chemical processes. Blended elemental technique (BE) The traditional technique of titanium production is via the Kroll process which involves chlorination of TiO2 ore in the presence of carbon and reacting the resulting TiCl4 with magnesium to produce titanium sponge. These processes take place at temperatures as ...
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Titanium
Titanium is a chemical element; it has symbol Ti and atomic number 22. Found in nature only as an oxide, it can be reduced to produce a lustrous transition metal with a silver color, low density, and high strength, resistant to corrosion in sea water, aqua regia, and chlorine. Titanium was discovered in Cornwall, Great Britain, by William Gregor in 1791 and was named by Martin Heinrich Klaproth after the Titans of Greek mythology. The element occurs within a number of minerals, principally rutile and ilmenite, which are widely distributed in the Earth's crust and lithosphere; it is found in almost all living things, as well as bodies of water, rocks, and soils. The metal is extracted from its principal mineral ores by the Kroll and Hunter processes. The most common compound, titanium dioxide (TiO2), is a popular photocatalyst and is used in the manufacture of white pigments. Other compounds include titanium tetrachloride (TiCl4), a component of smoke screens and cata ...
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Coatings
A coating is a covering that is applied to the surface of an object, or substrate. The purpose of applying the coating may be decorative, functional, or both. Coatings may be applied as liquids, gases or solids e.g. powder coatings. Paints and lacquers are coatings that mostly have dual uses, which are protecting the substrate and being decorative, although some artists paints are only for decoration, and the paint on large industrial pipes is for identification (e.g. blue for process water, red for fire-fighting control) in addition to preventing corrosion. Along with corrosion resistance, functional coatings may also be applied to change the surface properties of the substrate, such as adhesion, wettability, or wear resistance.Howarth G.A "Synthesis of a legislation compliant corrosion protection coating system based on urethane, oxazolidine and waterborne epoxy technology" Master of Science Thesis April 1997 Imperial College London In other cases the coating adds a comple ...
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Titanium Sponge Plant
Titanium Sponge Plant is an Indian manufacturing plant that produces titanium sponge, a material widely used in aeronautics, light defence vehicles, and other applications. It is located at Kerala Minerals and Metals Ltd ( KMML), Chavara, Kollam district of Kerala. Notably, It is the only plant in the world that carries out the entire aerospace-grade titanium sponge manufacturing process under one roof. History The importance of establishing domestic titanium production was realised due to India's significant demand for titanium and magnesium alloys, which were predominantly imported from countries such as China, Russia, and Japan. Dr. APJ Abdul Kalam, a scientist and the former President of India, highlighted the issue in a speech at the Kerala Legislative Assembly. The plant was fully commissioned in August 2015. Establishment The successful implementation was achieved after about twenty years of continuous research by the Defence Metallurgical Research Laboratory ( DMRL under ...
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Spark Plasma Sintering
Spark plasma sintering (SPS), also known as field assisted sintering technique (FAST) or pulsed electric current sintering (PECS), or plasma pressure compaction (P2C) is a sintering technique. The main characteristic of SPS is that the pulsed or unpulsed DC or AC current directly passes through the graphite die, as well as the powder compact, in case of conductive samples. Joule heating has been found to play a dominant role in the densification of powder compacts, which results in achieving near theoretical density at lower sintering temperature compared to conventional sintering techniques. The heat generation is internal, in contrast to the conventional hot pressing, where the heat is provided by external heating elements. This facilitates a very high heating or cooling rate (up to 1000 K/min), hence the sintering process generally is very fast (within a few minutes). The general speed of the process ensures it has the potential of densifying powders with nanosize or nanostruc ...
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Selective Laser Sintering
Selective laser sintering (SLS) is an additive manufacturing (AM) technique that uses a laser as the power and heat source to sinter powdered material (typically nylon or polyamide), aiming the laser automatically at points in space defined by a 3D model, binding the material together to create a solid structure. It is similar to selective laser melting; the two are instantiations of the same concept but differ in technical details. SLS (as well as the other mentioned AM techniques) is a relatively new technology that so far has mainly been used for rapid prototyping and for low-volume production of component parts. Production roles are expanding as the commercialization of AM technology improves. History Selective laser sintering (SLS) was developed and patented by Dr. Carl Deckard and academic adviser, Dr. Joe Beaman at the University of Texas at Austin in the mid-1980s, under sponsorship of DARPA. Deckard and Beaman were involved in the resulting start up company Des ...
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Niobium
Niobium is a chemical element; it has chemical symbol, symbol Nb (formerly columbium, Cb) and atomic number 41. It is a light grey, crystalline, and Ductility, ductile transition metal. Pure niobium has a Mohs scale of mineral hardness, Mohs hardness rating similar to pure titanium, and it has similar ductility to iron. Niobium oxidizes in Earth's atmosphere very slowly, hence its application in jewelry as a hypoallergenic alternative to nickel. Niobium is often found in the minerals pyrochlore and columbite. Its name comes from Greek mythology: Niobe, daughter of Tantalus, the namesake of tantalum. The name reflects the great similarity between the two elements in their physical and chemical properties, which makes them difficult to distinguish. English chemist Charles Hatchett reported a new element similar to tantalum in 1801 and named it columbium. In 1809, English chemist William Hyde Wollaston wrongly concluded that tantalum and columbium were identical. German chemist He ...
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Kroll Process
The Kroll process is a pyrometallurgical industrial process used to produce metallic titanium from titanium tetrachloride. As of 2001 William Justin Kroll's process replaced the Hunter process for almost all commercial production. Process In the Kroll process, titanium tetrachloride is reduced by liquid magnesium to give titanium metal: : + 2 ->[825~^\mathrm] + 2 The reduction is conducted at 800–850 °C in a stainless steel retort. Complications result from partial reduction of the TiCl4, giving to the lower chlorides Titanium(II) chloride, TiCl2 and Titanium(III) chloride, TiCl3. The magnesium chloride, MgCl2 can be further refined back to magnesium. Appurtenant processes The resulting porous metallic titanium sponge is purified by Tank leaching, leaching or vacuum distillation. The sponge is crushed, and pressed before it is melted in a consumable electrode vacuum Electric arc furnace, arc furnace, "backfilled with pure gettered argon of a pressure high enough to avoi ...
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Catalyst
Catalysis () is the increase in rate of a chemical reaction due to an added substance known as a catalyst (). Catalysts are not consumed by the reaction and remain unchanged after it. If the reaction is rapid and the catalyst recycles quickly, very small amounts of catalyst often suffice; mixing, surface area, and temperature are important factors in reaction rate. Catalysts generally react with one or more reactants to form intermediates that subsequently give the final reaction product, in the process of regenerating the catalyst. The rate increase occurs because the catalyst allows the reaction to occur by an alternative mechanism which may be much faster than the noncatalyzed mechanism. However the noncatalyzed mechanism does remain possible, so that the total rate (catalyzed plus noncatalyzed) can only increase in the presence of the catalyst and never decrease. Catalysis may be classified as either homogeneous, whose components are dispersed in the same phase (usual ...
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Powder Metallurgy
Powder metallurgy (PM) is a term covering a wide range of ways in which materials or components are made from metal powders. PM processes are sometimes used to reduce or eliminate the need for subtractive manufacturing, subtractive processes in manufacturing, lowering material losses and reducing the cost of the final product. This occurs especially often with small metal parts, like gears for small machines. Some porous products, allowing liquid or gas to permeate them, are produced in this way. They are also used when melting a material is impractical, due to it having a high melting point, or an alloy of two mutually insoluble materials, such as a mixture of copper and graphite. In this way, powder metallurgy can be used to make unique materials impossible to get from melting or forming in other ways. A very important product of this type is tungsten carbide. Tungsten carbide is used to cut and form other metals and is made from tungsten carbide particles bonded with cobalt. Tu ...
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Near Net Shape
Near-net-shape is an industrial manufacturing technique. As the name implies, the initial production of the item is very close to the final, or ''net'', shape. This reduces the need for surface finishing. By minimizing the use of finishing methods like machining or grinding, near-net-shape production eliminates more than two-thirds of the production costs in some industries. Processes The following are various near-net-shape processes categorized by material. Ceramics * Gelcasting * Ceramic injection molding * Spray forming *Structural ceramic production Composites * Lanxide process Plastics *Injection moulding *Rapid prototyping Metals *Casting ** Permanent mold casting *Powder metallurgy * Linear friction welding * Friction welding * Metal injection molding *Rapid prototyping * Spray forming * Superplastic forming *Cold forming * Semi-solid metal casting *Photochemical machining Photochemical machining (PCM), also known as photochemical milling or photo etching, is a che ...
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3D Printing
3D printing, or additive manufacturing, is the construction of a three-dimensional object from a CAD model or a digital 3D model. It can be done in a variety of processes in which material is deposited, joined or solidified under computer control, with the material being added together (such as plastics, liquids or powder grains being fused), typically layer by layer. In the 1980s, 3D printing techniques were considered suitable only for the production of functional or aesthetic prototypes, and a more appropriate term for it at the time was rapid prototyping. , the precision, repeatability, and material range of 3D printing have increased to the point that some 3D printing processes are considered viable as an industrial-production technology; in this context, the term ''additive manufacturing'' can be used synonymously with ''3D printing''. One of the key advantages of 3D printing is the ability to produce very complex shapes or geometries that would be otherwise infeasi ...
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Medical Implants
An implant is a medical device manufactured to replace a missing biological structure, support a damaged biological structure, or enhance an existing biological structure. For example, an implant may be a rod, used to strengthen weak bones. Medical implants are human-made devices, in contrast to a transplant, which is a transplanted biomedical tissue. The surface of implants that contact the body might be made of a biomedical material such as titanium, silicone, or apatite depending on what is the most functional. In 2018, for example, American Elements developed a nickel alloy powder for 3D printing robust, long-lasting, and biocompatible medical implants. In some cases implants contain electronics, e.g. artificial pacemaker and cochlear implants. Some implants are bioactive, such as subcutaneous drug delivery devices in the form of implantable pills or drug-eluting stents. Applications Implants can roughly be categorized into groups by application: Sensory and neurolog ...
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