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Precession Electron Diffraction
Precession electron diffraction (PED) is a specialized method to collect electron diffraction patterns in a transmission electron microscope (TEM). By rotating (precessing) a tilted incident electron beam around the central axis of the microscope, a PED pattern is formed by integration over a collection of diffraction conditions. This produces a quasi-kinematical diffraction pattern that is more suitable as input into direct methods (crystallography), direct methods algorithms to determine the crystal structure of the sample. Overview Geometry Precession electron diffraction is accomplished utilizing the standard instrument configuration of a modern Transmission electron microscope, TEM. The animation illustrates the geometry used to generate a PED pattern. Specifically, the beam tilt coils located pre-specimen are used to tilt the electron beam off of the optic axis so it is incident with the specimen at an angle, φ. The image shift coils post-specimen are then used to til ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Bragg Condition
In many areas of science, Bragg's law — also known as Georg Wulff, Wulff–Bragg's condition or Laue–Bragg interference — is a special case of Laue diffraction that gives the angles for coherent scattering of waves from a large crystal lattice. It describes how the superposition of wave fronts scattered by lattice planes leads to a strict relation between the wavelength and scattering angle. This law was initially formulated for X-rays, but it also applies to all types of Matter wave, matter waves including neutron and electron waves if there are a large number of atoms, as well as to visible light with artificial periodic microscale lattices. History Bragg diffraction (also referred to as the Bragg formulation of X-ray diffraction) was first proposed by Lawrence Bragg and his father, William Henry Bragg, in 1913 after their discovery that crystalline solids produced surprising patterns of reflected X-rays (in contrast to those produced with, for instance, a liquid). They ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Crystal System
In crystallography, a crystal system is a set of point groups (a group of geometric symmetries with at least one fixed point). A lattice system is a set of Bravais lattices (an infinite array of discrete points). Space groups (symmetry groups of a configuration in space) are classified into crystal systems according to their point groups, and into lattice systems according to their Bravais lattices. Crystal systems that have space groups assigned to a common lattice system are combined into a crystal family. The seven crystal systems are ''triclinic'', ''monoclinic'', ''orthorhombic'', ''tetragonal'', ''trigonal'', ''hexagonal'', and ''cubic''. Informally, two crystals are in the same crystal system if they have similar symmetries (though there are many exceptions). Classifications Crystals can be classified in three ways: lattice systems, crystal systems and crystal families. The various classifications are often confused: in particular the trigonal crystal system i ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Crystal Symmetry
In crystallography, crystal structure is a description of ordered arrangement of atoms, ions, or molecules in a crystalline material. Ordered structures occur from intrinsic nature of constituent particles to form symmetric patterns that repeat along the principal directions of three-dimensional space in matter. The smallest group of particles in a material that constitutes this repeating pattern is the unit cell of the structure. The unit cell completely reflects the symmetry and structure of the entire crystal, which is built up by repetitive translation of the unit cell along its principal axes. The translation vectors define the nodes of the Bravais lattice. The lengths of principal axes/edges, of the unit cell and angles between them are lattice constants, also called ''lattice parameters'' or ''cell parameters''. The symmetry properties of a crystal are described by the concept of space groups. All possible symmetric arrangements of particles in three-dimensional space ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Mechanical Properties
A material property is an intensive property of a material, i.e., a physical property or chemical property that does not depend on the amount of the material. These quantitative properties may be used as a metric by which the benefits of one material versus another can be compared, thereby aiding in materials selection. A property having a fixed value for a given material or substance is called material constant or constant of matter. (Material constants should not be confused with physical constants, that have a universal character.) A material property may also be a function of one or more independent variables, such as temperature. Materials properties often vary to some degree according to the direction in the material in which they are measured, a condition referred to as anisotropy. Materials properties that relate to different physical phenomena often behave linearly (or approximately so) in a given operating range . Modeling them as linear functions can significantly si ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Electromagnetic
In physics, electromagnetism is an interaction that occurs between particles with electric charge via electromagnetic fields. The electromagnetic force is one of the four fundamental forces of nature. It is the dominant force in the interactions of atoms and molecules. Electromagnetism can be thought of as a combination of electrostatics and magnetism, which are distinct but closely intertwined phenomena. Electromagnetic forces occur between any two charged particles. Electric forces cause an attraction between particles with opposite charges and repulsion between particles with the same charge, while magnetism is an interaction that occurs between charged particles in relative motion. These two forces are described in terms of electromagnetic fields. Macroscopic charged objects are described in terms of Coulomb's law for electricity and Ampère's force law for magnetism; the Lorentz force describes microscopic charged particles. The electromagnetic force is responsible for ma ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Electronic Band Structure
In solid-state physics, the electronic band structure (or simply band structure) of a solid describes the range of energy levels that electrons may have within it, as well as the ranges of energy that they may not have (called ''band gaps'' or ''forbidden bands''). Band theory derives these bands and band gaps by examining the allowed quantum mechanical wave functions for an electron in a large, periodic lattice of atoms or molecules. Band theory has been successfully used to explain many physical properties of solids, such as electrical resistivity and optical absorption, and forms the foundation of the understanding of all solid-state devices (transistors, solar cells, etc.). Why bands and band gaps occur The formation of electronic bands and band gaps can be illustrated with two complementary models for electrons in solids. The first one is the nearly free electron model, in which the electrons are assumed to move almost freely within the material. In this model, the ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Electron Crystallography
Electron crystallography is a subset of methods in electron diffraction focusing upon detailed determination of the positions of atoms in solids using a transmission electron microscope (TEM). It can involve the use of high-resolution transmission electron microscopy images, electron diffraction patterns including convergent-beam electron diffraction or combinations of these. It has been successful in determining some bulk structures, and also surface structures. Two related methods are low-energy electron diffraction which has solved the structure of many surfaces, and reflection high-energy electron diffraction which is used to monitor surfaces often during growth. The technique date back to soon after the discovery of electron diffraction in 1927-28, and was used in many early works. However, for many years quantitative electron crystallography was not used, instead the diffraction information was combined qualitatively with imaging results. A number of advances from the 195 ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
X-ray Crystallography
X-ray crystallography is the experimental science of determining the atomic and molecular structure of a crystal, in which the crystalline structure causes a beam of incident X-rays to Diffraction, diffract in specific directions. By measuring the angles and intensities of the X-ray diffraction, a crystallography, crystallographer can produce a three-dimensional picture of the density of electrons within the crystal and the positions of the atoms, as well as their chemical bonds, crystallographic disorder, and other information. X-ray crystallography has been fundamental in the development of many scientific fields. In its first decades of use, this method determined the size of atoms, the lengths and types of chemical bonds, and the atomic-scale differences between various materials, especially minerals and alloys. The method has also revealed the structure and function of many biological molecules, including vitamins, drugs, proteins and nucleic acids such as DNA. X-ray crystall ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Crystallography
Crystallography is the branch of science devoted to the study of molecular and crystalline structure and properties. The word ''crystallography'' is derived from the Ancient Greek word (; "clear ice, rock-crystal"), and (; "to write"). In July 2012, the United Nations recognised the importance of the science of crystallography by proclaiming 2014 the International Year of Crystallography.UN announcement "International Year of Crystallography" iycr2014.org. 12 July 2012 Crystallography is a broad topic, and many of its subareas, such as X-ray crystallography, are themselves important scientific topics. Crystallography ranges from the fundamentals of crystal structure to the mathematics of Crystal system, crystal geometry, including those that are Aperiodic crystal, not periodic or quasi ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Jon Gjønnes
Jon Kjell Gjønnes (26 January 1931 – 6 April 2021) was a Norwegian physicist. Career Born in Brevik, Gjønnes graduated as cand. real. from the University of Oslo in 1957, and as dr.philos. in 1967. He was appointed professor at the University of Oslo in 1982. His research contributions were mainly in the fields of x-ray diffraction, electron diffraction and electron microscopy. In 2008 he was the inaugural recipient of a medal for outstanding contribution to the Field of Electron crystallography, from the International Union of Crystallography; the medal was named the ''Gjønnes Medal'' in his honour. He was a fellow of the Norwegian Academy of Science and Letters from 1987. Gjønnes was also an elected member of Bærum municipal council and from 1979 to 1981 a political adviser in Nordli's Cabinet Nordli's Cabinet governed Norway between 15 January 1976 and 4 February 1981. The Labour Party cabinet was led by Odvar Nordli Odvar Nordli (; 3 November 1926 – 9 Janua ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Paul Midgley
Paul Anthony Midgley (born 1966) FRS is a Professor of Materials Science in the Department of Materials Science and Metallurgy at the University of Cambridge and a fellow of Peterhouse, Cambridge. Education Midgley was educated at the University of Bristol where he was awarded a Master of Science degree in 1988 and a PhD in 1991 for work on electron microscopy of high-temperature superconductors. Career Before moving to Cambridge in 1997, Midgley held two postdoctoral research fellowships in the Henry Herbert Wills Physics Laboratory at the University of Bristol. Research Midgley's research interests are in electron tomography, electron holography, energy-filtered imaging and ''ab initio'' structure determination by electron diffraction. During his research, Midgley has collaborated with Mark Welland, Rafal Dunin-Borkowski, Neil Mathur, John Meurig Thomas, Brian F. G. Johnson and Henning Sirringhaus. Midgley's research has been funded by the Engineering and Physical Sc ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
