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Ground Glass Joint
Ground glass joints are used in laboratories to quickly and easily fit leak-tight apparatus together from interchangeable commonly available parts. For example, a round bottom flask, Liebig condenser, and oil bubbler with ground glass joints may be rapidly fitted together to reflux a reaction mixture. This is a large improvement compared with older methods of custom-made glassware, which was time-consuming and expensive, or the use of less chemical resistant and heat resistant corks or rubber bungs and glass tubes as joints, which took time to prepare as well. One of the glassware items to be joined would have an ''inner'' (or male) ''joint'' with the ground glass surface facing outward and the other would have an ''outer'' (or female) ''joint'' of a correspondingly fitting taper with the ground glass surface facing inward. To connect the hollow inner spaces of the glassware components, ground glass joints are hollow on the inside and open at the ends, except for stoppers ...
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Round Bottom Flask
Round-bottom flasks (also called round-bottomed flasks or RB flasks) are types of flasks having spherical bottoms used as laboratory glassware, mostly for chemical or biochemical work. They are typically made of glass for chemical inertness; and in modern days, they are usually made of heat-resistant borosilicate glass. There is at least one tubular section known as the ''neck'' with an opening at the tip. Two- or three-necked flasks are common as well. Round bottom flasks come in many sizes, from 5 mL to 20 L, with the sizes usually inscribed on the glass. In pilot plants even larger flasks are encountered. The ends of the necks are usually conical ground glass joints. These are standardized, and can accept any similarly-sized tapered (male) fittings. 24/20 is common for 250 mL or larger flasks, while smaller sizes such as 14/20 or 19/22 are used for smaller flasks. Because of the round bottom, cork rings are needed to keep the round bottom flasks upright. ...
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Laboratory Glassware
Laboratory glassware refers to a variety of equipment used in scientific work, and traditionally made of glass. Glass can be blown, bent, cut, molded, and formed into many sizes and shapes, and is therefore common in chemistry, biology, and analytical laboratories. Many laboratories have training programs to demonstrate how glassware is used and to alert first–time users to the safety hazards involved with using glassware. History Ancient era The history of glassware dates back to the Phoenicians who fused obsidian together in campfires making the first glassware. Glassware evolved as other ancient civilizations including the Syrians, Egyptians, and Romans refined the art of glassmaking. Mary the Jewess, an alchemist in Alexandria during the 1st century AD, is credited for the creation of some of the first glassware for chemical such as the ''kerotakis'' which was used for the collection of fumes from a heated material. Despite these creations, glassware for chemical ...
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Perfluoroisobutylene
Perfluoroisobutene (PFIB) is the perfluorocarbon counterpart of the hydrocarbon isobutene and has the formula (CF3)2C=CF2. An alkene, it is a colorless gas that is notable as a highly toxic perfluoroalkene. Few simple alkenes are as toxic. Safety Perfluoroisobutene is quite toxic with an LCt = 880 mg⋅min⋅m−3 (mice). It is a Schedule 2 substance of the Chemical Weapons Convention. Perfluoroisobutene is highly reactive toward nucleophiles. It hydrolyzes readily to give the relatively innocuous (CF3)2CHCO2H, which readily decarboxylates to give hexafluoropropane. It forms addition compounds with thiols, and it is this reactivity that may be related to its toxicity. PFIB is a product of pyrolysis of polytetrafluoroethylene (PTFE), one of the substances invoked to explain polymer fume fever. External links International Chemical Safety Card 1216 See also *Phosgene Phosgene is the organic chemical compound with the formula COCl2. It is a toxic, colorless gas; in ...
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Polyacetal
Polyoxymethylene (POM), also known as acetal, polyacetal, and polyformaldehyde, is an engineering thermoplastic used in precision parts requiring high stiffness, low friction, and excellent dimensional stability. As with many other synthetic polymers, it is produced by different chemical firms with slightly different formulas and sold variously by such names as Delrin, Kocetal, Ultraform, Celcon, Ramtal, Duracon, Kepital, Polypenco, Tenac and Hostaform. POM is characterized by its high strength, hardness and rigidity to −40 °C. POM is intrinsically opaque white because of its high crystalline composition but can be produced in a variety of colors. POM has a density of 1.410–1.420g/cm3. Typical applications for injection-molded POM include high-performance engineering components such as small gear wheels, eyeglass frames, ball bearings, ski bindings, fasteners, gun parts, knife handles, and lock systems. The material is widely used in the automotive and consume ...
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Hermann Keck
Hermann Keck (1919 – 2010) was a German scientist who invented the Keck Clip. Keck was born in Treysa Treysa, an independent town until 1970, is the biggest ''Stadtteil'' of the German town Schwalmstadt. It was incorporated into Schwalmstadt in December 1970. The location around Treysa and Schwalmstadt is called Schwalm. The historic city lies ... and has two patents on his name: * Clip for fixing male and female parts of ground glass joints, (1984). * Handled clamp for ground glass ball and socket joints or the like, (1988).Design patent References {{DEFAULTSORT:Keck, Hermann 20th-century German chemists 1919 births 2010 deaths People from Schwalmstadt 20th-century German inventors ...
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Keck Clips
Ground glass joints are used in laboratories to quickly and easily fit leak-tight apparatus together from interchangeable commonly available parts. For example, a round bottom flask, Liebig condenser, and oil bubbler with ground glass joints may be rapidly fitted together to reflux a reaction mixture. This is a large improvement compared with older methods of custom-made glassware, which was time-consuming and expensive, or the use of less chemical resistant and heat resistant corks or rubber bungs and glass tubes as joints, which took time to prepare as well. One of the glassware items to be joined would have an ''inner'' (or male) ''jo