Vacuum drying is the

mass transfer Mass transfer is the net movement of mass from one location (usually meaning stream, phase, fraction, or component) to another. Mass transfer occurs in many processes, such as absorption, evaporation, drying, precipitation, membrane filtra ...

operation in which the moisture present in a substance, usually a wet solid, is removed by means of creating a

vacuum A vacuum (: vacuums or vacua) is space devoid of matter. The word is derived from the Latin adjective (neuter ) meaning "vacant" or "void". An approximation to such vacuum is a region with a gaseous pressure much less than atmospheric pressur ...

. In chemical processing industries like

food processing Food processing is the transformation of agricultural products into food, or of one form of food into other forms. Food processing takes many forms, from grinding grain into raw flour, home cooking, and complex industrial methods used in the mak ...

, pharmacology, agriculture, and textiles, drying is an essential unit operation to remove moisture. Vacuum drying is generally used for the drying of substances that are

hygroscopic Hygroscopy is the phenomenon of attracting and holding water molecules via either absorption (chemistry), absorption or adsorption from the surrounding Natural environment, environment, which is usually at normal or room temperature. If water mol ...

and heat-sensitive, and is based on the principle of creating a vacuum to decrease the chamber pressure below the vapor pressure of the water, causing it to boil. With the help of vacuum pumps, the pressure is reduced around the substance to be dried. This decreases the

boiling point The boiling point of a substance is the temperature at which the vapor pressure of a liquid equals the pressure surrounding the liquid and the liquid changes into a vapor. The boiling point of a liquid varies depending upon the surrounding envi ...

of water inside that product and thereby increases the rate of

evaporation Evaporation is a type of vaporization that occurs on the Interface (chemistry), surface of a liquid as it changes into the gas phase. A high concentration of the evaporating substance in the surrounding gas significantly slows down evapora ...

significantly. The result is a significantly increased drying rate of the product. The vacuum drying process is a batch operation performed at reduced pressures and lower

relative humidity Humidity is the concentration of water vapor present in the air. Water vapor, the gaseous state of water, is generally invisible to the human eye. Humidity indicates the likelihood for precipitation (meteorology), precipitation, dew, or fog t ...

compared to ambient pressure, enabling faster drying.

Vacuum dryer

Vacuum dryer is the equipment with the help of which vacuum drying is carried out. Vacuum dryers are sometimes made up of cast iron, but most are made of stainless steel, so that they can bear the high vacuum pressure without any kind of deformation. The oven is divided into hollow trays which increases the surface area for

heat conduction Thermal conduction is the diffusion of thermal energy (heat) within one material or between materials in contact. The higher temperature object has molecules with more kinetic energy; collisions between molecules distributes this kinetic energy u ...

. The oven door is locked air tight and is connected to vacuum pump to reduce the pressure. The materials to be dried are kept on the trays inside the vacuum dryer and pressure is reduced by means of a vacuum pump. The dryer door is tightly shut and steam is passed through the space between trays and jacket so that the heat transfer occurs by conduction. Water vapors from the feed is sent into the condenser and after the drying vacuum pump is disconnected and the dried product is collected from the trays.

Microwave vacuum drying

Because conventional drying approaches (e.g., convective drying) may cause great nutritional and textural changes (like a darker color due to Maillard reaction), microwave vacuum drying is an alternative for pharmaceuticals and food drying, a method known since 1989. The microwaves speed up the drying process and lower temperature in vacuum system, reducing overall drying cycle time and temperature-induced effects of the food product. Microwave vacuum drying may be used for production of dried pharmaceuticals and food. Industrialized equipment, however, may require pre-treating samples before processing in the industrial vacuum system; pre-drying is used by conventional methods to reduce bulk water content.

Applications

Vacuum dryer can be used to dry heat sensitive hygroscopic and toxic materials. If the feed for drying is a solution, it can be dried using vacuum dryer as the solvent can be recovered by condensation. To improve the quality of products, such as for fruit preservation, hybrid drying combining osmotic dehydration followed by

heat pump A heat pump is a device that uses electricity to transfer heat from a colder place to a warmer place. Specifically, the heat pump transfers thermal energy using a heat pump and refrigeration cycle, cooling the cool space and warming the warm s ...

drying and

microwave Microwave is a form of electromagnetic radiation with wavelengths shorter than other radio waves but longer than infrared waves. Its wavelength ranges from about one meter to one millimeter, corresponding to frequency, frequencies between 300&n ...

-vacuum drying proved effective.

References

{{Reflist Drying