Soil Samples
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A soil test is a
laboratory A laboratory (; ; colloquially lab) is a facility that provides controlled conditions in which scientific or technological research, experiments, and measurement may be performed. Laboratories are found in a variety of settings such as schools ...
or
in-situ is a Latin phrase meaning 'in place' or 'on site', derived from ' ('in') and ' ( ablative of ''situs'', ). The term typically refers to the examination or occurrence of a process within its original context, without relocation. The term is use ...
analysis to determine the chemical, physical or biological characteristics of a soil. Possibly the most widely conducted soil tests are those performed to estimate the plant-available concentrations of
nutrients A nutrient is a substance used by an organism to survive, grow and reproduce. The requirement for dietary nutrient intake applies to animals, plants, fungi and protists. Nutrients can be incorporated into cells for metabolic purposes or excret ...
in order to provide
fertilizer A fertilizer or fertiliser is any material of natural or synthetic origin that is applied to soil or to plant tissues to supply plant nutrients. Fertilizers may be distinct from liming materials or other non-nutrient soil amendments. Man ...
recommendations in agriculture. In
geotechnical engineering Geotechnical engineering, also known as geotechnics, is the branch of civil engineering concerned with the engineering behavior of earth materials. It uses the principles of soil mechanics and rock mechanics to solve its engineering problems. I ...
, soil tests can be used to determine the current physical state of the soil, the
seepage In soil mechanics, seepage is the movement of water through soil. If fluid pressures in a soil deposit are uniformly increasing with depth according to u = \rho_w g z_w, where z_w is the depth below the water table, then hydrostatic conditions wi ...
properties, the
shear strength In engineering, shear strength is the strength of a material or component against the type of yield or structural failure when the material or component fails in shear. A shear load is a force that tends to produce a sliding failure on a mater ...
and the deformation properties of the soil. Other soil tests may be used in
geochemical Geochemistry is the science that uses the tools and principles of chemistry to explain the mechanisms behind major geological systems such as the Earth's crust and its oceans. The realm of geochemistry extends beyond the Earth, encompassing the ...
or
ecological Ecology () is the natural science of the relationships among living organisms and their environment. Ecology considers organisms at the individual, population, community, ecosystem, and biosphere levels. Ecology overlaps with the closely re ...
investigations.


Agricultural soil tests

In
agriculture Agriculture encompasses crop and livestock production, aquaculture, and forestry for food and non-food products. Agriculture was a key factor in the rise of sedentary human civilization, whereby farming of domesticated species created ...
, a soil test commonly refers to the
analysis Analysis (: analyses) is the process of breaking a complex topic or substance into smaller parts in order to gain a better understanding of it. The technique has been applied in the study of mathematics and logic since before Aristotle (38 ...
of a
soil Soil, also commonly referred to as earth, is a mixture of organic matter, minerals, gases, water, and organisms that together support the life of plants and soil organisms. Some scientific definitions distinguish dirt from ''soil'' by re ...
sample to determine
nutrient A nutrient is a substance used by an organism to survive, grow and reproduce. The requirement for dietary nutrient intake applies to animals, plants, fungi and protists. Nutrients can be incorporated into cells for metabolic purposes or excret ...
content, composition, and other characteristics such as the
acidity An acid is a molecule or ion capable of either donating a proton (i.e. hydrogen cation, H+), known as a Brønsted–Lowry acid, or forming a covalent bond with an electron pair, known as a Lewis acid. The first category of acids are the ...
or pH level. A soil test can determine
fertility Fertility in colloquial terms refers the ability to have offspring. In demographic contexts, fertility refers to the actual production of offspring, rather than the physical capability to reproduce, which is termed fecundity. The fertility rate ...
, or the expected growth potential of the soil which indicates nutrient deficiencies, potential toxicities from excessive fertility and inhibitions from the presence of non-essential
trace mineral __NOTOC__ A trace element is a chemical element of a minute quantity, a trace amount, especially used in referring to a micronutrient, but is also used to refer to minor elements in the composition of a rock, or other chemical substance. In nutri ...
s. The test is used to mimic the function of roots to assimilate minerals. The expected rate of growth is modeled by the Law of the Maximum. Labs, such as those at Iowa State and
Colorado State University Colorado State University (Colorado State or CSU) is a Public university, public Land-grant university, land-grant research university in Fort Collins, Colorado, United States. It is the flagship university of the Colorado State University Syst ...
, recommend that a soil test contains 10-20 sample points for every of field.
Tap water Tap water (also known as running water, piped water or municipal water) is water supplied through a Tap (valve), tap, a water dispenser valve. In many countries, tap water usually has the quality of drinking water. Tap water is commonly used f ...
or chemicals can change the composition of the soil, and may need to be tested separately. As soil nutrients vary with depth and soil components change with time, the depth and timing of a sample may also affect results. Composite sampling can be performed by combining soil from several locations prior to analysis. This is a common procedure, but should be used judiciously to avoid skewing results. This procedure must be done so that government sampling requirements are met. A reference map should be created to record the location and quantity of field samples in order to properly interpret test results.


Geographic distribution of samples for precision agriculture

In
precision agriculture Precision agriculture (PA) is a management strategy that gathers, processes and analyzes temporal, spatial and individual plant and animal data and combines it with other information to support management decisions according to estimated varia ...
, soil samples may be geolocated using GPS technology in order to estimate the geospatial distribution of nutrients in the sampled area. The geolocated samples are collected using a distribution and resolution that allows for the estimation of the geospatial variability of the soil area where the crop will be grown. Many different distributions and resolutions are used, depending upon many factors including the goals of the geospatial nutrient analysis and cost of sample collection and analysis. For example, in the United States corn and soybean growing regions a grid distribution with a resolution of 2.5 acres per grid (one sample for each 2.5 acre grid) is offered by many precision agriculture soil test service providers. This is generally referred to as grid soil testing.


Storage, handling, and moving

Soil chemistry changes over time, as biological and which chemical processes break down or combine compounds over time. These processes change once the soil is removed from its natural ecosystem (flora and fauna that penetrate the sampled area) and environment (temperature, moisture, and solar light/radiation cycles). As a result, the chemical composition analysis accuracy can be improved if the soil is analyzed soon after its extraction — usually within a relative time period of 24 hours. The chemical changes in the soil can be slowed during storage and transportation by freezing it. Air drying can also preserve the soil sample for many months.


Lab testing

Soil testing is often performed by commercial labs that offer a variety of tests, targeting groups of compounds and minerals. Laboratory tests often check for plant nutrients in three categories: * Major nutrients:
nitrogen Nitrogen is a chemical element; it has Symbol (chemistry), symbol N and atomic number 7. Nitrogen is a Nonmetal (chemistry), nonmetal and the lightest member of pnictogen, group 15 of the periodic table, often called the Pnictogen, pnictogens. ...
,
phosphorus Phosphorus is a chemical element; it has Chemical symbol, symbol P and atomic number 15. All elemental forms of phosphorus are highly Reactivity (chemistry), reactive and are therefore never found in nature. They can nevertheless be prepared ar ...
, and
potassium Potassium is a chemical element; it has Symbol (chemistry), symbol K (from Neo-Latin ) and atomic number19. It is a silvery white metal that is soft enough to easily cut with a knife. Potassium metal reacts rapidly with atmospheric oxygen to ...
* Secondary nutrients:
sulfur Sulfur ( American spelling and the preferred IUPAC name) or sulphur ( Commonwealth spelling) is a chemical element; it has symbol S and atomic number 16. It is abundant, multivalent and nonmetallic. Under normal conditions, sulfur atoms ...
,
calcium Calcium is a chemical element; it has symbol Ca and atomic number 20. As an alkaline earth metal, calcium is a reactive metal that forms a dark oxide-nitride layer when exposed to air. Its physical and chemical properties are most similar to it ...
,
magnesium Magnesium is a chemical element; it has Symbol (chemistry), symbol Mg and atomic number 12. It is a shiny gray metal having a low density, low melting point and high chemical reactivity. Like the other alkaline earth metals (group 2 ...
* Minor nutrients:
iron Iron is a chemical element; it has symbol Fe () and atomic number 26. It is a metal that belongs to the first transition series and group 8 of the periodic table. It is, by mass, the most common element on Earth, forming much of Earth's o ...
,
manganese Manganese is a chemical element; it has Symbol (chemistry), symbol Mn and atomic number 25. It is a hard, brittle, silvery metal, often found in minerals in combination with iron. Manganese was first isolated in the 1770s. It is a transition m ...
,
copper Copper is a chemical element; it has symbol Cu (from Latin ) and atomic number 29. It is a soft, malleable, and ductile metal with very high thermal and electrical conductivity. A freshly exposed surface of pure copper has a pinkish-orang ...
,
zinc Zinc is a chemical element; it has symbol Zn and atomic number 30. It is a slightly brittle metal at room temperature and has a shiny-greyish appearance when oxidation is removed. It is the first element in group 12 (IIB) of the periodic tabl ...
,
boron Boron is a chemical element; it has symbol B and atomic number 5. In its crystalline form it is a brittle, dark, lustrous metalloid; in its amorphous form it is a brown powder. As the lightest element of the boron group it has three ...
,
molybdenum Molybdenum is a chemical element; it has Symbol (chemistry), symbol Mo (from Neo-Latin ''molybdaenum'') and atomic number 42. The name derived from Ancient Greek ', meaning lead, since its ores were confused with lead ores. Molybdenum minerals hav ...
,
chlorine Chlorine is a chemical element; it has Symbol (chemistry), symbol Cl and atomic number 17. The second-lightest of the halogens, it appears between fluorine and bromine in the periodic table and its properties are mostly intermediate between ...
The amount of plant-available
phosphorus Phosphorus is a chemical element; it has Chemical symbol, symbol P and atomic number 15. All elemental forms of phosphorus are highly Reactivity (chemistry), reactive and are therefore never found in nature. They can nevertheless be prepared ar ...
is most often measured with a chemical extraction method, and different countries have different standard methods. Just in Europe, more than 10 different soil phosphorus tests are currently in use and the results from these different tests are not directly comparable.
Do-it-yourself "Do it yourself" ("DIY") is the method of building, modifying, or repairing things by oneself without the direct aid of professionals or certified experts. Academic research has described DIY as behaviors where "individuals use raw and semi- ...
kits usually only test for the three "major nutrients", and for soil
acidity An acid is a molecule or ion capable of either donating a proton (i.e. hydrogen cation, H+), known as a Brønsted–Lowry acid, or forming a covalent bond with an electron pair, known as a Lewis acid. The first category of acids are the ...
or pH level. Do-it-yourself kits are often sold at farming cooperatives, university labs, private labs, and some hardware and gardening stores.
Electrical meter North American domestic analog ( Ferraris disk) electricity meter. Electricity meter with transparent plastic case (Israel) Electricity meter in West Bengal, IndiaAn electricity meter, electric meter, electrical meter, energy meter, or kil ...
s that measure pH, water content, and sometimes nutrient content of the soil are also available at many hardware stores. Laboratory tests are more accurate than tests with do-it-yourself kits and electrical meters. A
example soil sample report
is provided for reference by Wallace Laboratories LLC. In order to avoid complex and expensive analytical techniques, prediction based on regression equations relating to more easily measurable parameters can be provided by pedotransfer functions. For instance, soil bulk density can be predicted using easily measured soil properties such as soil texture, pH and organic matter. Soil testing is used to facilitate fertilizer composition and dosage selection for land employed in both agricultural and horticultural industries. Prepaid mail-in kits for soil and ground water testing are available to facilitate the packaging and delivery of samples to a laboratory. Similarly, in 2004, laboratories began providing fertilizer recommendations along with the soil composition report. Lab tests are more accurate and often utilize very precise flow injection technology (or Near InfraRed (NIR) scanning). In addition, lab tests frequently include professional interpretation of results and recommendations. Provisory statements included in a lab report may outline any anomalies, exceptions, and shortcomings in the sampling, analytical process or results. Some laboratories analyze for all 13 mineral nutrients and a dozen non-essential, potentially toxic minerals utilizing the "universal soil extractant" (
ammonium bicarbonate Ammonium bicarbonate is an inorganic compound with formula (NH4)HCO3. The compound has many names, reflecting its long history. Chemically speaking, it is the bicarbonate salt of the ammonium ion. It is a colourless solid that degrades readily to ...
DTPA).


Engineering soil testing

In
geotechnical engineering Geotechnical engineering, also known as geotechnics, is the branch of civil engineering concerned with the engineering behavior of earth materials. It uses the principles of soil mechanics and rock mechanics to solve its engineering problems. I ...
, a soil test can be used to determine the physical characteristics of a soil, such as its
water content Water content or moisture content is the quantity of water contained in a material, such as soil (called ''soil moisture''), rock, ceramics, crops, or wood. Water content is used in a wide range of scientific and technical areas, and is expressed ...
, void ratio or
bulk density In materials science, bulk density, also called apparent density, is a material property defined as the mass of the many particles of the material divided by the bulk volume. Bulk volume is defined as the total volume the particles occupy, includ ...
. Soil testing can also provide information related to the
shear strength In engineering, shear strength is the strength of a material or component against the type of yield or structural failure when the material or component fails in shear. A shear load is a force that tends to produce a sliding failure on a mater ...
, rate of consolidation and permeability of the soil. The following is a non-exhaustive list of engineering soil tests.


Soil contaminants

Common mineral soil contaminants include
arsenic Arsenic is a chemical element; it has Symbol (chemistry), symbol As and atomic number 33. It is a metalloid and one of the pnictogens, and therefore shares many properties with its group 15 neighbors phosphorus and antimony. Arsenic is not ...
,
barium Barium is a chemical element; it has symbol Ba and atomic number 56. It is the fifth element in group 2 and is a soft, silvery alkaline earth metal. Because of its high chemical reactivity, barium is never found in nature as a free element. Th ...
,
cadmium Cadmium is a chemical element; it has chemical symbol, symbol Cd and atomic number 48. This soft, silvery-white metal is chemically similar to the two other stable metals in group 12 element, group 12, zinc and mercury (element), mercury. Like z ...
,
copper Copper is a chemical element; it has symbol Cu (from Latin ) and atomic number 29. It is a soft, malleable, and ductile metal with very high thermal and electrical conductivity. A freshly exposed surface of pure copper has a pinkish-orang ...
, mercury,
lead Lead () is a chemical element; it has Chemical symbol, symbol Pb (from Latin ) and atomic number 82. It is a Heavy metal (elements), heavy metal that is density, denser than most common materials. Lead is Mohs scale, soft and Ductility, malleabl ...
, and
zinc Zinc is a chemical element; it has symbol Zn and atomic number 30. It is a slightly brittle metal at room temperature and has a shiny-greyish appearance when oxidation is removed. It is the first element in group 12 (IIB) of the periodic tabl ...
. Lead is a particularly dangerous soil component. The following table from the
University of Minnesota The University of Minnesota Twin Cities (historically known as University of Minnesota) is a public university, public Land-grant university, land-grant research university in the Minneapolis–Saint Paul, Twin Cities of Minneapolis and Saint ...
categorizes typical soil concentration levels and their associated health risks. The following is a non-exhaustive list of recommendations to limit exposure to lead in garden soils: # Locate gardens away from old painted structures and heavily traveled roads # Give planting preferences to fruiting crops (tomatoes, squash, peas, sunflowers, corn, etc.) # Incorporate organic materials such as finished
compost Compost is a mixture of ingredients used as plant fertilizer and to improve soil's physical, chemical, and biological properties. It is commonly prepared by Decomposition, decomposing plant and food waste, recycling organic materials, and man ...
, humus, and peat moss # Lime soil as recommended by soil test (a pH of 6.5 minimizes lead availability) # Discard old and outer leaves before eating leafy vegetables; peel root crops; wash all produce # Keep dust to a minimum by maintaining a mulched and/or moist soil surface


See also

* Base-cation saturation ratio *
Fertilizer A fertilizer or fertiliser is any material of natural or synthetic origin that is applied to soil or to plant tissues to supply plant nutrients. Fertilizers may be distinct from liming materials or other non-nutrient soil amendments. Man ...
*
Geotechnical investigation Geotechnical investigations are performed by geotechnical engineers or engineering geologists to obtain information on the physical properties of soil earthworks and foundations for proposed structures and for repair of distress to earthworks ...
*
Liming (soil) Liming is the application of calcium- (Ca) and magnesium (Mg)-rich materials in various forms, including marl, chalk, limestone, burnt lime or hydrated lime to soil. In acid soils, these materials react as a base and neutralize soil acidity. T ...
* Plant tissue test * SESL Australia


References


External links


Pollutants/Toxics > Soil Contaminants





Mail-in soil test kits and nutrient management/fertilizer reports

Field Book for Describing and Sampling Soils
{{Authority control In situ geotechnical investigations