
A florentine flask, also known as florentine receiver, florentine separator or essencier (from the French), other shapes called florentine vase or florentine vessel, is an
oil–water separator fed with condensed vapors of a steam distillation in a
fragrance extraction process.
Description
When the raw material is heated with steam from boiling water, volatile fragrant compounds and steam leave the
still. The vapours are cooled in the
condenser and become liquid. The liquid runs into the florentine receiver where the water and essential oil phases separate.
The essential oils phase separates from water because the oils have a different density than water, and are not water-soluble.
There are two main types of florentines in use. One separates essential oils of lower density than water, for example
lavender oil, accumulating in a layer floating on the water.
This kind of florentine has to be airtight to reduce the loss of volatile substances.
The other type is intended for oils that are denser than water, where the oil accumulates beneath the water phase, for instance
cinnamon
Cinnamon is a spice obtained from the inner bark of several tree species from the genus ''Cinnamomum''. Cinnamon is used mainly as an aromatic condiment and flavouring additive in a wide variety of cuisines, sweet and savoury dishes, breakfa ...
,
wintergreen,
vetiver,
patchouli or
cloves
Cloves are the aromatic flower buds of a tree in the family Myrtaceae, ''Syzygium aromaticum'' (). They are native to the Maluku Islands (or Moluccas) in Indonesia, and are commonly used as a spice, flavoring or fragrance in consumer products, s ...
.
The floating water phase avoids the loss of volatile compounds from the oil.
There are also florentines that are able to accommodate oils that are denser or less dense than water.
The separated water is a
herbal distillate and can be fed back into the still or may in some cases be sold as herbal water.
Because small droplets of oil are entrained with the water flowing out of the florentine, the yield can sometimes be increased by using more than one florentine in series.
For laboratory use, a small glass florentine without a base is called a ''florentine vase'', as it has a slight resemblance to a small
amphora
An amphora (; grc, ἀμφορεύς, ''amphoreús''; English plural: amphorae or amphoras) is a type of container with a pointed bottom and characteristic shape and size which fit tightly (and therefore safely) against each other in storag ...
. Larger glass receivers with base are called ''florentine flasks'' or ''essenciers''.
Glass is normally only used up to 15 liter vessels; above this size, glass is too fragile, so that metal is used for larger capacities.
References
{{Reflist
Essential oils
Flavor technology
Liquid-liquid separation
Distillation