|
Sub-sampling (chemistry)
In analytical chemistry, sub-sampling is a procedure by which a small, representative sample is taken from a larger sample. Good sub-sampling technique becomes important when the large sample is not homogeneous. Techniques Coning and quartering Coning and quartering is a method used by analytical chemists to reduce the sample size of a powder without creating a systematic bias. The technique involves pouring the sample so that it takes on a conical shape, and then flattening it out into a cake. The cake is then divided into quarters; the two quarters which sit opposite one another are discarded, while the other two are combined and constitute the reduced sample. The same process is continued until an appropriate sample size remains. Analyses are made with respect to the sample left behind. Riffle box splitting A riffle box is a box containing a number (between 3 and 12) of "chutes" - slotted paths through which particles of the sample may slide. The sample is dropped into th ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Analytical Chemistry
Analytical skill, Analytical chemistry studies and uses instruments and methods to Separation process, separate, identify, and Quantification (science), quantify matter. In practice, separation, identification or quantification may constitute the entire analysis or be combined with another method. Separation isolates analytes. Qualitative inorganic analysis, Qualitative analysis identifies analytes, while Quantitative analysis (chemistry), quantitative analysis determines the numerical amount or concentration. Analytical chemistry consists of classical, wet chemistry, wet chemical methods and modern analytical techniques. Classical qualitative methods use separations such as Precipitation (chemistry), precipitation, Extraction (chemistry), extraction, and distillation. Identification may be based on differences in color, odor, melting point, boiling point, solubility, radioactivity or reactivity. Classical quantitative analysis uses mass or volume changes to quantify amount. Ins ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Representative Sample
In this statistics, quality assurance, and survey methodology, sampling is the selection of a subset or a statistical sample (termed sample for short) of individuals from within a statistical population to estimate characteristics of the whole population. The subset is meant to reflect the whole population, and statisticians attempt to collect samples that are representative of the population. Sampling has lower costs and faster data collection compared to recording data from the entire population (in many cases, collecting the whole population is impossible, like getting sizes of all stars in the universe), and thus, it can provide insights in cases where it is infeasible to measure an entire population. Each observation measures one or more properties (such as weight, location, colour or mass) of independent objects or individuals. In survey sampling, weights can be applied to the data to adjust for the sample design, particularly in stratified sampling. Results from probab ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Homogeneous (chemistry)
In chemistry, a mixture is a material made up of two or more different chemical substances which can be separated by physical method. It is an impure substance made up of 2 or more elements or compounds mechanically mixed together in any proportion. A mixture is the physical combination of two or more substances in which the identities are retained and are mixed in the form of Solution (chemistry), solutions, Suspension (chemistry), suspensions or colloids. Mixtures are one product of mechanically blending or mixing chemical substances such as chemical element, elements and Compound (chemistry), compounds, without chemical bonding or other chemical change, so that each ingredient substance retains its own chemical properties and makeup. Despite the fact that there are no chemical changes to its constituents, the physical properties of a mixture, such as its melting point, may differ from those of the components. Some mixtures can be separation process, separated into their compone ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Sample (material)
In general, a sample is a limited quantity of something which is intended to be similar to and represent a larger amount of that thing(s). The things could be Count noun, countable objects such as individual items available as units for sale, or an Mass noun, uncountable material. Even though the word "sample" implies a smaller quantity taken from a larger amount, sometimes full Biological specimen, biological or Type specimen (mineralogy), mineralogical specimens are called samples if they are taken for analysis, testing, or investigation like other samples. They are also considered samples in the sense that even whole specimens are "samples" of the full population of many individual organisms. The act of obtaining a sample is called "sampling" and can be performed manually by a person or by automatic process. Samples of material can be taken or provided for testing, Analyser, analysis, investigation, Acceptance sampling, quality control, demonstration, or trial use. Sometime ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Powder (substance)
A powder is a dry solid composed of many very fine particles that may flow freely when shaken or tilted. Powders are a special sub-class of granular materials, although the terms ''powder'' and ''granular'' are sometimes used to distinguish separate classes of material. In particular, ''powders'' refer to those granular materials that have the finer grain sizes, and that therefore have a greater tendency to form clumps when flowing. ''Granulars'' refer to the coarser granular materials that do not tend to form clumps except when wet. Types Many manufactured goods come in powder form, such as flour, sugar, ground coffee, powdered milk, copy machine toner, gunpowder, cosmetic powders, and some pharmaceuticals. In nature, dust, fine sand and snow, volcanic ash, and the top layer of the lunar regolith are also examples. Because of their importance to industry, medicine and earth science, powders have been studied in great detail by chemical engineers, mechanical engineers ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Systematic Error
Observational error (or measurement error) is the difference between a measurement, measured value of a physical quantity, quantity and its unknown true value.Dodge, Y. (2003) ''The Oxford Dictionary of Statistical Terms'', OUP. Such errors are inherent in the measurement process; for example lengths measured with a ruler calibrated in whole centimeters will have a measurement error of several millimeters. The error or uncertainty of a measurement can be estimated, and is specified with the measurement as, for example, 32.3 ± 0.5 cm. Scientific observations are marred by two distinct types of errors, systematic errors on the one hand, and Statistical randomness, random, on the other hand. The effects of random errors can be mitigated by the repeated measurements. Constant or systematic errors on the contrary must be carefully avoided, because they arise from one or more causes which constantly act in the same way, and have the effect of always altering the result of the experi ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Riffle Splitter
The riffle splitter is a device used to divide a bulk sample of material into smaller, representative sub-samples. It can be used in laboratory settings or fieldwork. The device is usually constructed with steel sheet and should be designed to have an even number of opposing inclined chutes (the riffles), with each chute having the same width. The recommended chute width should be at least 2.5× the size of the maximum particle diameter that can be found in the lot to be split. Riffle splitters are typically used in assay and analytical laboratories to reduce the size of samples provided from other sources (crushed rock, soils, powders and so on) to a lot size that is appropriate for the next stage of analytical sample preparation. Design There are many different versions of the riffle splitter. However, not all can be considered correct sub-sampling devices, in that the two sub-sample halves are deemed to be representative of the original lot. The issue of correctness of a rif ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Mining
Mining is the Resource extraction, extraction of valuable geological materials and minerals from the surface of the Earth. Mining is required to obtain most materials that cannot be grown through agriculture, agricultural processes, or feasibly created Chemical synthesis, artificially in a laboratory or factory. Ores recovered by mining include Metal#Extraction, metals, coal, oil shale, gemstones, limestone, chalk mining, chalk, dimension stone, rock salt, potash, gravel, and clay. The ore must be a rock or mineral that contains valuable constituent, can be extracted or mined and sold for profit. Mining in a wider sense includes extraction of any non-renewable resource such as petroleum, natural gas, or even fossil water, water. Modern mining processes involve prospecting for ore bodies, analysis of the profit potential of a proposed mine, extraction of the desired materials, and final mine reclamation, reclamation or restoration of the land after the mine is closed. Mining ma ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Assaying
An assay is an investigative (analytic) procedure in laboratory medicine, mining, pharmacology, environmental biology and molecular biology for qualitatively assessing or quantitatively measuring the presence, amount, or functional activity of a target entity. The measured entity is often called the analyte, the measurand, or the target of the assay. The analyte can be a drug, biochemical substance, chemical element or compound, or cell in an organism or organic sample. An assay usually aims to measure an analyte's intensive property and express it in the relevant measurement unit (e.g. molarity, density, functional activity in enzyme international units, degree of effect in comparison to a standard, etc.). If the assay involves exogenous reactants (the reagents), then their quantities are kept fixed (or in excess) so that the quantity and quality of the target are the only limiting factors. The difference in the assay outcome is used to deduce the unknown quality or quantity ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
