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Oil Bubbler
A gas bubbler is a piece of laboratory glassware which consists of a glass bulb filled with a small amount of fluid—usually mineral oil, mineral or silicone oil, less commonly mercury. The inlet to the bulb is connected to a ground glass joint, while the outlet is vented to the air. Gas bubblers are used to exclude air from a reaction or a system. In the former case, the gas bubbler is fitted on the Condenser (laboratory), condenser of the reaction set-up. In the latter case, an oil bubbler is usually installed at the end of the inert gas manifold on a Schlenk line to prevent contamination by atmospheric oxygen and water. A gas bubbler acts as a one-way valve—gases (hot air, evolved gases, solvent vapors) from the inlet will bubble through the fluid before being vented to the atmosphere. If there were an underpressure in the reaction vessel (such as when heat is removed, and the gases within contract), some fluid is sucked into a sump to equalize the pressure, inst ...
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Cannula Transfer
Cannula transfer or cannulation is a set of air-free techniques used with a Schlenk line, in transferring liquid or solution samples between reaction vessels via cannulae, avoiding atmospheric contamination. Syringes are not the same as cannulae, but cannula transfer techniques remain relevant when using them for this purpose. Two methods of cannula transfer are popular: vacuum, and pressure. Both utilize differences in pressures between two vessels to push the fluid through. Often, the main difficulty encountered is slow transfer due to the high viscosity of the fluid. Equipment Septa Septa (: septum) are rubber stoppers which seal flasks or bottles. They give an airtight seal, preventing the ingress of the atmosphere, but are able to be pierced by sharp needles or cannulae. Cannula Cannulae are hollow flexible tubes. Their bore is usually 16-22 gauge thick. They are commonly made of stainless steel or PTFE for their chemical resistance. Stainless steel cannulae are usually 2� ...
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Drying Tube
A drying tube or guard tube is a tube-like piece of apparatus used to house a disposable solid desiccant, wherein at one end the tube-like structure terminates in a ground glass joint for use in connecting the drying tube to a reaction vessel, for the purpose of keeping the vessel free of moisture. The tube-like structure is often bent and can also widen to form a bulb/desiccant reservoir. Typically a drying tube is 1–2 cm wide and 5–10 cm long and bent at an angle of about 90 degrees. In use, the drying tube is filled with a rechargeable desiccant such as calcium chloride, and the open end of drying tube is partially blocked (e.g. with wool, glasswool or a bung/cork which has a small bore made in it) and the drying tube is connected to the apparatus to be kept dry via the ground glass joint. If the drying tube is bent the bend is oriented so that solid desiccant does not fall into the reaction vessel. Some drying tubes have a glass sinter to prevent desiccant fall ...
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Avantor
Avantor, Inc. is an American biotechnology, chemicals, and pharmaceutical company headquartered in Radnor, Pennsylvania. Established in 1904 as ''J.T. Baker'', the company changed its name to ''Avantor'' in 2010. Avantor went public in 2019 and is now listed on the New York Stock Exchange under the symbol “AVTR”. History The company's history traces back to 1904, when John Townsend Baker (1860-1935) founded the chemical company J.T. Baker specializing in producing chemically pure reagents. The company gained recognition for its "Baker Analyzed" labels, which provided detailed analyses of trace impurities in its products. In 1911, the company began publishing "The Chemist-Analyst," which promoted its products and philosophy. After Baker's death in 1935, the company was acquired by Vick Chemical Company in 1941. During World War II, J.T. Baker expanded its product line to include penicillin, pesticides, and chemicals for batteries and munitions. After the war, the company furt ...
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Acetylenes
\ce \ce Acetylene \ce \ce \ce Propyne \ce \ce \ce \ce 1-Butyne In organic chemistry, an alkyne is an unsaturated hydrocarbon containing at least one carbon—carbon triple bond. The simplest acyclic alkynes with only one triple bond and no other functional groups form a homologous series with the general chemical formula . Alkynes are traditionally known as acetylenes, although the name ''acetylene'' also refers specifically to , known formally as ethyne using IUPAC nomenclature. Like other hydrocarbons, alkynes are generally hydrophobic. Structure and bonding In acetylene, the H–C≡C bond angles are 180°. By virtue of this bond angle, alkynes are rod-like. Correspondingly, cyclic alkynes are rare. Benzyne cannot be isolated. The C≡C bond distance of 118 picometers (for C2H2) is much shorter than the C=C distance in alkenes (132 pm, for C2H4) or the C–C bond in alkanes (153 pm). : The triple bond is very strong with a bond strength of 839 kJ/mol. The si ...
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Ammonia
Ammonia is an inorganic chemical compound of nitrogen and hydrogen with the chemical formula, formula . A Binary compounds of hydrogen, stable binary hydride and the simplest pnictogen hydride, ammonia is a colourless gas with a distinctive pungent smell. It is widely used in fertilizers, refrigerants, explosives, cleaning agents, and is a precursor for numeous chemicals. Biologically, it is a common nitrogenous waste, and it contributes significantly to the nutritional needs of terrestrial organisms by serving as a precursor to fertilisers. Around 70% of ammonia produced industrially is used to make fertilisers in various forms and composition, such as urea and diammonium phosphate. Ammonia in pure form is also applied directly into the soil. Ammonia, either directly or indirectly, is also a building block for the synthesis of many chemicals. In many countries, it is classified as an List of extremely hazardous substances, extremely hazardous substance. Ammonia is toxic, cau ...
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Sintered Glass
Fritted glass is finely porous glass through which gas or liquid may pass, made by sintering together glass particles into a solid but porous body. This porous glass body can also be called a frit. Applications in laboratory glassware include use in fritted glass filter items, scrubbers, or spargers. Other laboratory applications of fritted glass include packing in chromatography columns and resin beds for special chemical synthesis. In a fritted glass filter, a disc or pane of fritted glass is used to filter out solid particles, precipitate, or residue from a fluid, similar to a piece of filter paper. The fluid can go through the pores in the fritted glass, but the frit will often stop a solid from going through. A fritted filter is often part of a glassware item, so fritted glass funnels and fritted glass crucibles are available. Laboratory scale spargers (also known as gas diffusing stones or diffusors) as well as scrubber Scrubber systems (e.g. chemical scrubbe ...
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Mercury (element)
Mercury is a chemical element; it has Symbol (chemistry), symbol Hg and atomic number 80. It is commonly known as quicksilver. A Heavy metal element, heavy, silvery d-block element, mercury is the only metallic element that is known to be liquid at standard temperature and pressure; the only other element that is liquid under these conditions is the halogen bromine, though metals such as caesium, gallium, and rubidium melt just above room temperature. Mercury occurs in deposits throughout the world mostly as cinnabar (mercuric sulfide). The red pigment vermilion is obtained by Mill (grinding), grinding natural cinnabar or synthetic mercuric sulfide. Exposure to mercury and mercury-containing organic compounds is toxic to the nervous system, immune system and kidneys of humans and other animals; mercury poisoning can result from exposure to water-soluble forms of mercury (such as mercuric chloride or methylmercury) either directly or through mechanisms of biomagnification. Mercu ...
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Air Sensitive Cannula - No Bleed Valve
An atmosphere () is a layer of gases that envelop an astronomical object, held in place by the gravity of the object. A planet retains an atmosphere when the gravity is great and the temperature of the atmosphere is low. A stellar atmosphere is the outer region of a star, which includes the layers above the opaque photosphere; stars of low temperature might have outer atmospheres containing compound molecules. The atmosphere of Earth is composed of nitrogen (78%), oxygen (21%), argon (0.9%), carbon dioxide (0.04%) and trace gases. Most organisms use oxygen for respiration; lightning and bacteria perform nitrogen fixation which produces ammonia that is used to make nucleotides and amino acids; plants, algae, and cyanobacteria use carbon dioxide for photosynthesis. The layered composition of the atmosphere minimises the harmful effects of sunlight, ultraviolet radiation, solar wind, and cosmic rays and thus protects the organisms from genetic damage. The current composition of t ...
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Water
Water is an inorganic compound with the chemical formula . It is a transparent, tasteless, odorless, and Color of water, nearly colorless chemical substance. It is the main constituent of Earth's hydrosphere and the fluids of all known living organisms (in which it acts as a solvent). It is vital for all known forms of life, despite not providing food energy or organic micronutrients. Its chemical formula, , indicates that each of its molecules contains one oxygen and two hydrogen atoms, connected by covalent bonds. The hydrogen atoms are attached to the oxygen atom at an angle of 104.45°. In liquid form, is also called "water" at standard temperature and pressure. Because Earth's environment is relatively close to water's triple point, water exists on Earth as a solid, a liquid, and a gas. It forms precipitation in the form of rain and aerosols in the form of fog. Clouds consist of suspended droplets of water and ice, its solid state. When finely divided, crystalline ice ...
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Oxygen
Oxygen is a chemical element; it has chemical symbol, symbol O and atomic number 8. It is a member of the chalcogen group (periodic table), group in the periodic table, a highly reactivity (chemistry), reactive nonmetal (chemistry), nonmetal, and a potent oxidizing agent that readily forms oxides with most elements as well as with other chemical compound, compounds. Oxygen is abundance of elements in Earth's crust, the most abundant element in Earth's crust, making up almost half of the Earth's crust in the form of various oxides such as water, carbon dioxide, iron oxides and silicates.Atkins, P.; Jones, L.; Laverman, L. (2016).''Chemical Principles'', 7th edition. Freeman. It is abundance of chemical elements, the third-most abundant element in the universe after hydrogen and helium. At standard temperature and pressure, two oxygen atoms will chemical bond, bind covalent bond, covalently to form dioxygen, a colorless and odorless diatomic gas with the chemical formula ...
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