Vacuum Filtration
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Vacuum Filtration
Vacuum filtration is a fast filtration technique used to separate solids from liquids. Principle By flowing through the aspirator, water will suck out the air contained in the vacuum flask and the Büchner flask. There is therefore a difference in pressure between the exterior and the interior of the flasks : the contents of the Büchner funnel are sucked towards the vacuum flask. The filter, which is placed at the bottom of the Büchner funnel, separates the solids from the liquids. The solid residue, which remains at the top of the Büchner funnel, is therefore recovered more efficiently: it is much drier than it would be with a simple filtration. The rubber conical seal ensures the apparatus is hermetically closed, preventing the passage of air between the Büchner funnel and the vacuum flask. It maintains the vacuum in the apparatus and also avoids physical points of stress (glass against glass.) Diagram annotations # Filter # Büchner funnel # Conic seal # Büchner flask ...
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Vacuum
A vacuum (: vacuums or vacua) is space devoid of matter. The word is derived from the Latin adjective (neuter ) meaning "vacant" or "void". An approximation to such vacuum is a region with a gaseous pressure much less than atmospheric pressure. Physicists often discuss ideal test results that would occur in a ''perfect'' vacuum, which they sometimes simply call "vacuum" or free space, and use the term partial vacuum to refer to an actual imperfect vacuum as one might have in a laboratory or in space. In engineering and applied physics on the other hand, vacuum refers to any space in which the pressure is considerably lower than atmospheric pressure. The Latin term ''in vacuo'' is used to describe an object that is surrounded by a vacuum. The ''quality'' of a partial vacuum refers to how closely it approaches a perfect vacuum. Other things equal, lower gas pressure means higher-quality vacuum. For example, a typical vacuum cleaner produces enough suction to reduce air pressur ...
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Filtration
Filtration is a physical separation process that separates solid matter and fluid from a mixture using a ''filter medium'' that has a complex structure through which only the fluid can pass. Solid particles that cannot pass through the filter medium are described as ''oversize'' and the fluid that passes through is called the ''filtrate''. Oversize particles may form a filter cake on top of the filter and may also block the filter lattice, preventing the fluid phase from crossing the filter, known as ''blinding''. The size of the largest particles that can successfully pass through a filter is called the effective ''pore size'' of that filter. The separation of solid and fluid is imperfect; solids will be contaminated with some fluid and filtrate will contain fine particles (depending on the pore size, filter thickness and biological activity). Filtration occurs both in nature and in engineered systems; there are biological, geological, and industrial forms. In everyday us ...
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Solid
Solid is a state of matter where molecules are closely packed and can not slide past each other. Solids resist compression, expansion, or external forces that would alter its shape, with the degree to which they are resisted dependent upon the specific material under consideration. Solids also always possess the least amount of kinetic energy per atom/molecule relative to other phases or, equivalently stated, solids are formed when matter in the liquid / gas phase is cooled below a certain temperature. This temperature is called the melting point of that substance and is an intrinsic property, i.e. independent of how much of the matter there is. All matter in solids can be arranged on a microscopic scale under certain conditions. Solids are characterized by structural rigidity and resistance to applied external forces and pressure. Unlike liquids, solids do not flow to take on the shape of their container, nor do they expand to fill the entire available volume like a gas. Much ...
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Liquid
Liquid is a state of matter with a definite volume but no fixed shape. Liquids adapt to the shape of their container and are nearly incompressible, maintaining their volume even under pressure. The density of a liquid is usually close to that of a solid, and much higher than that of a gas. Therefore, liquid and solid are classified as condensed matter. Meanwhile, since both liquids and gases can flow, they are categorized as fluids. A liquid is composed of atoms or molecules held together by intermolecular bonds of intermediate strength. These forces allow the particles to move around one another while remaining closely packed. In contrast, solids have particles that are tightly bound by strong intermolecular forces, limiting their movement to small vibrations in fixed positions. Gases, on the other hand, consist of widely spaced, freely moving particles with only weak intermolecular forces. As temperature increases, the molecules in a liquid vibrate more intensely, causi ...
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Aspirator (pump)
A vacuum ejector, or simply ejector, or aspirator, is a type of vacuum pump, which produces vacuum by means of the Venturi effect. In an ejector, a working fluid (liquid or gaseous) flows through a jet nozzle into a tube that first narrows and then expands in cross-sectional area. The fluid leaving the jet is flowing at a high velocity which due to Bernoulli's principle results in it having low pressure, thus generating a vacuum. The outer tube then narrows into a mixing section where the high velocity working fluid mixes with the fluid that is drawn in by the vacuum, imparting enough velocity for it to be ejected, the tube then typically expands in order to decrease the velocity of the ejected stream, allowing the pressure to smoothly increase to the external pressure. The strength of the vacuum produced depends on the velocity and shape of the fluid jet and the shape of the constriction and mixing sections, but if a liquid is used as the working fluid, the strength of the va ...
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Water
Water is an inorganic compound with the chemical formula . It is a transparent, tasteless, odorless, and Color of water, nearly colorless chemical substance. It is the main constituent of Earth's hydrosphere and the fluids of all known living organisms (in which it acts as a solvent). It is vital for all known forms of life, despite not providing food energy or organic micronutrients. Its chemical formula, , indicates that each of its molecules contains one oxygen and two hydrogen atoms, connected by covalent bonds. The hydrogen atoms are attached to the oxygen atom at an angle of 104.45°. In liquid form, is also called "water" at standard temperature and pressure. Because Earth's environment is relatively close to water's triple point, water exists on Earth as a solid, a liquid, and a gas. It forms precipitation in the form of rain and aerosols in the form of fog. Clouds consist of suspended droplets of water and ice, its solid state. When finely divided, crystalline ice ...
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Büchner Flask
A Büchner flask, also known as a vacuum flask,The use of the term ''vacuum flask'' sometimes causes confusion with the thermos flask filter flask, suction flask, side-arm flask, or Bunsen flask, is a thick-walled Erlenmeyer flask with a short glass tube and hose barb protruding about 1-2 cm from its neck. Description The short tube and hose barb effectively act as an adapter over which the end of a thick-walled hose can be fitted to form a connection to the flask. The other end of the hose can be connected to source of vacuum such as an aspirator, vacuum pump, or house vacuum. Preferably this is done through a trap (see below), which is designed to prevent the water to be sucked back from the aspirator into the Büchner flask. The purpose of applying a vacuum is to speed the filtration by providing a pressure differential across the filter medium that is greater than that produced by gravity alone. Operation The thick wall of the Büchner flask provides it the strength to withs ...
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Pressure
Pressure (symbol: ''p'' or ''P'') is the force applied perpendicular to the surface of an object per unit area over which that force is distributed. Gauge pressure (also spelled ''gage'' pressure)The preferred spelling varies by country and even by industry. Further, both spellings are often used ''within'' a particular industry or country. Industries in British English-speaking countries typically use the "gauge" spelling. is the pressure relative to the ambient pressure. Various #Units, units are used to express pressure. Some of these derive from a unit of force divided by a unit of area; the International System of Units, SI unit of pressure, the Pascal (unit), pascal (Pa), for example, is one newton (unit), newton per square metre (N/m2); similarly, the Pound (force), pound-force per square inch (Pound per square inch, psi, symbol lbf/in2) is the traditional unit of pressure in the imperial units, imperial and United States customary units, US customary systems. Pressure ma ...
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Büchner Funnel
A Büchner funnel is a piece of laboratory equipment used in filtration. It is traditionally made of porcelain, but glass and plastic funnels are also available. On top of the funnel-shaped part there is a cylinder with a fritted glass disc/perforated plate separating it from the funnel. The Hirsch funnel has a similar design; it is used similarly, but for smaller quantities of material. The main difference is that the plate of a Hirsch funnel is much smaller, and the walls of the funnel angle outward instead of being vertical. A funnel with a fritted glass disc can be used immediately. For a funnel with a perforated plate, filtration material in the form of filter paper is placed on the plate, and the filter paper is moistened with a liquid to prevent initial leakage. The liquid to be filtered is poured into the cylinder and drawn through the perforated plate/fritted glass disc by vacuum suction. The main advantage in using this type of filtration is that it proceeds much more ...
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Residue (chemistry)
In chemistry, residue is whatever remains or acts as a contaminant after a given class of events. Residue may be the material remaining after a process of preparation, separation, or purification, such as distillation, evaporation, or filtration. It may also denote the undesired by-products of a chemical reaction. Residues as an undesired by-product are a concern in agricultural and food industries. Food safety Toxic chemical residues, wastes or contamination from other processes, are a concern in food safety. The most common food residues originate from pesticides, veterinary drugs, and industrial chemicals. For example, the U.S. Food and Drug Administration (FDA) and the Canadian Food Inspection Agency (CFIA) have guidelines for detecting chemical residues that are possibly dangerous to consume. In the U.S., the FDA is responsible for setting guidelines while other organizations enforce them. Environmental concerns Similar to the food industry, in environmental science ...
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