Distillation Design
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''Distillation Design'' is a book which provides complete coverage of the design of industrial
distillation Distillation, or classical distillation, is the process of separating the components or substances from a liquid mixture by using selective boiling and condensation, usually inside an apparatus known as a still. Dry distillation is the he ...
column A column or pillar in architecture and structural engineering is a structural element that transmits, through compression (physical), compression, the weight of the structure above to other structural elements below. In other words, a column i ...
s for the
petroleum refining An oil refinery or petroleum refinery is an industrial process plant where petroleum (crude oil) is transformed and refined into useful products such as gasoline (petrol), diesel fuel, asphalt base, fuel oils, heating oil, kerosene, liquefi ...
,
chemical A chemical substance is a form of matter having constant chemical composition and characteristic properties. Some references add that chemical substance cannot be separated into its constituent elements by physical separation methods, i.e., w ...
and
petrochemical Petrochemicals (sometimes abbreviated as petchems) are the chemical products obtained from petroleum by refining. Some chemical compounds made from petroleum are also obtained from other fossil fuels, such as coal or natural gas, or renewabl ...
plants,
natural gas processing Natural-gas processing is a range of industrial processes designed to purify raw natural gas by removing impurities, contaminants and higher molecular mass hydrocarbons to produce what is known as ''pipeline quality'' dry natural gas. Natural gas ...
,
pharmaceutical A medication (also called medicament, medicine, pharmaceutical drug, medicinal drug or simply drug) is a drug used to diagnose, cure, treat, or prevent disease. Drug therapy ( pharmacotherapy) is an important part of the medical field and ...
, food and alcohol distilling industries. It has been a classical
chemical engineering Chemical engineering is an engineering field which deals with the study of operation and design of chemical plants as well as methods of improving production. Chemical engineers develop economical commercial processes to convert raw materials in ...
textbook since it was first published in February 1992. The subjects covered in the book include: *''
Vapor–liquid equilibrium In thermodynamics and chemical engineering, the vapor–liquid equilibrium (VLE) describes the distribution of a chemical species between the vapor phase and a liquid phase. The concentration of a vapor in contact with its liquid, especially a ...
(VLE)'': Vapor–liquid K values, relative volatilities, ideal and non-ideal systems, phase diagrams, calculating bubble points and
dew point The dew point is the temperature to which air must be cooled to become saturated with water vapor, assuming constant air pressure and water content. When cooled below the dew point, moisture capacity is reduced and airborne water vapor will ...
s *''Key
fractional distillation Fractional distillation is the separation of a mixture into its component parts, or fractions. Chemical compounds are separated by heating them to a temperature at which one or more fractions of the mixture will vaporize. It uses distillation ...
concepts'': theoretical stages, x-y diagrams, multicomponent distillation, column composition and temperature profiles *'' Process design and
optimization Mathematical optimization (alternatively spelled ''optimisation'') or mathematical programming is the selection of a best element, with regard to some criterion, from some set of available alternatives. It is generally divided into two subfi ...
'': minimum
reflux Reflux is a technique involving the condensation of vapors and the return of this condensate to the system from which it originated. It is used in industrial and laboratory distillations. It is also used in chemistry to supply energy to reactions ...
and minimum stages, optimum reflux, short-cut methods, feed entry location *''Rigorous calculation methods'': Bubble point method, sum rates method, numerical methods (
Newton–Raphson In numerical analysis, Newton's method, also known as the Newton–Raphson method, named after Isaac Newton and Joseph Raphson, is a root-finding algorithm which produces successively better approximations to the roots (or zeroes) of a real-va ...
technique), inside out method, relaxation method, other methods *''
Batch distillation Batch distillation refers to the use of distillation in batches, meaning that a mixture is distilled to separate it into its component fractions before the distillation still is again charged with more mixture and the process is repeated. This is i ...
'': Simple distillation, constant reflux, varying reflux, time and boilup requirements *''Tray design and tray efficiency'': tray types, tray capacities, tray hydraulic parameters, tray sizing and determination of column diameter, point and tray efficiencies, tray efficiency prediction and scaleup *'' Packing design and packing efficiency'': packing types, packing hydraulics and capacities, determination of packing efficiency by transfer unit method and by
HETP A theoretical plate in many separation processes is a hypothetical zone or stage in which two phases, such as the liquid and vapor phases of a substance, establish an equilibrium with each other. Such equilibrium stages may also be referred to as ...
method, packed column sizing


See also

* * * * * * * *


External links


McGraw Hill website page
{dead link, date=December 2016 , bot=InternetArchiveBot , fix-attempted=yes Distillation Engineering textbooks Science books Technology books