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Retort
In a chemistry laboratory, a retort is a device used for distillation or dry distillation of substances. It consists of a spherical vessel with a long downward-pointing neck. The liquid to be distilled is placed in the vessel and heated. The neck acts as a condenser, allowing the vapors to condense and flow along the neck to a collection vessel placed underneath. In the chemical industry, a retort is an airtight vessel in which substances are heated for a chemical reaction producing gaseous products to be collected in a collection vessel or for further processing. Such industrial-scale retorts are used in shale oil extraction, the production of charcoal and in the recovery of mercury in gold mining processes and hazardous waste. A process of heating oil shale to produce shale oil, oil shale gas, and spent shale is commonly called retorting. Airtight vessels to apply pressure as well as heat are called autoclaves. In the food industry, pressure cookers are often referred t ...
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Shale Oil Extraction
Shale oil extraction is an industrial process for unconventional oil production. This process converts kerogen in oil shale into shale oil by pyrolysis, hydrogenation, or thermal dissolution. The resultant shale oil is used as fuel oil or upgraded to meet refinery feedstock specifications by adding hydrogen and removing sulfur and nitrogen impurities. Shale oil extraction is usually performed above ground (''ex situ'' processing) by mining the oil shale and then treating it in processing facilities. Other modern technologies perform the processing underground (on-site or ''in situ'' processing) by applying heat and extracting the oil via oil wells. The earliest description of the process dates to the 10th century. In 1684, Great Britain granted the first formal extraction process patent. Extraction industries and innovations became widespread during the 19th century. The industry shrank in the mid-20th century following the discovery of large reserves of conventional oil, ...
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Retort Pouch
A retort pouch or retortable pouch is a type of food packaging made from a laminate of flexible plastic and metal foils. It allows the sterile packaging of a wide variety of food and drink handled by aseptic processing, and is used as an alternative to traditional industrial canning methods. Packaged foods range from water to fully cooked, thermo-stabilized (heat-treated) high-caloric (1,300 kcal on average) meals such as Meals, Ready-to-Eat (MREs), which can be eaten cold, warmed by submersing in hot water, or through the use of a flameless ration heater, a meal component introduced by the military in 1992. Retort pouches are used in field rations, space food, fish products, camping food, instant noodles, and brands such as Capri Sun and Tasty Bite. Some varieties have a bottom gusset and are known as stand-up pouches. Origin The retort pouch was invented by the United States Army Natick R&D Command, Reynolds Metals Company, and Continental Flexible Packaging, who jointly ...
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Oil Shale
Oil shale is an organic-rich fine-grained sedimentary rock containing kerogen (a solid mixture of organic chemical compounds) from which liquid hydrocarbons can be produced. In addition to kerogen, general composition of oil shales constitutes inorganic substance and bitumens. Based on their deposition environment, oil shales are classified as marine, lacustrine and terrestrial oil shales. Oil shales differ from oil-''bearing'' shales, shale deposits that contain petroleum ( tight oil) that is sometimes produced from drilled wells. Examples of oil-''bearing'' shales are the Bakken Formation, Pierre Shale, Niobrara Formation, and Eagle Ford Formation. Accordingly, shale oil produced from oil shale should not be confused with tight oil, which is also frequently called shale oil. Deposits of oil shale occur around the world, including major deposits in the United States. A 2016 estimate of global deposits set the total world resources of oil shale equivalent of of oil in pla ...
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Liebig Condenser
The Liebig condenser (, ) or straight condenser is a piece of laboratory equipment, specifically a condenser consisting of a straight glass tube surrounded by a water jacket. In typical laboratory operation, such as distillation, the condenser is clamped to a retort stand in vertical or oblique orientation. The hot vapor of some liquid is introduced at the upper end of the inner tube, and condenses in contact with its colder walls. Water (or some other fluid) is constantly circulated in the jacket to carry away the heat of vaporization released by the condensing vapor, keeping the tube below the liquid's boiling point. The condensed liquid drips out of the lower end of the inner tube. The Liebig condenser can also be used in reflux or Soxhlet extraction operations, although other condenser types are better suited to those tasks. In this usage, the condenser is held vertically above the recipient with the boiling liquid. The vapor is admitted to the inner tube through the lo ...
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Distillation
Distillation, or classical distillation, is the process of separating the components or substances from a liquid mixture by using selective boiling and condensation, usually inside an apparatus known as a still. Dry distillation is the heating of solid materials to produce gaseous products (which may condense into liquids or solids); this may involve chemical changes such as destructive distillation or cracking. Distillation may result in essentially complete separation (resulting in nearly pure components), or it may be a partial separation that increases the concentration of selected components; in either case, the process exploits differences in the relative volatility of the mixture's components. In industrial applications, distillation is a unit operation of practically universal importance, but is a physical separation process, not a chemical reaction. An installation used for distillation, especially of distilled beverages, is a distillery. Distillation includes ...
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Distillation By Retort
Distillation, or classical distillation, is the process of separating the components or substances from a liquid mixture by using selective boiling and condensation, usually inside an apparatus known as a still. Dry distillation is the heating of solid materials to produce gaseous products (which may condense into liquids or solids); this may involve chemical changes such as destructive distillation or cracking. Distillation may result in essentially complete separation (resulting in nearly pure components), or it may be a partial separation that increases the concentration of selected components; in either case, the process exploits differences in the relative volatility of the mixture's components. In industrial applications, distillation is a unit operation of practically universal importance, but is a physical separation process, not a chemical reaction. An installation used for distillation, especially of distilled beverages, is a distillery. Distillation includes the ...
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Shale Oil
Shale oil is an unconventional oil produced from oil shale rock fragments by pyrolysis, hydrogenation, or thermal dissolution. These processes convert the organic matter within the rock ( kerogen) into synthetic oil and gas. The resulting oil can be used immediately as a fuel or upgraded to meet refinery feedstock specifications by adding hydrogen and removing impurities such as sulfur and nitrogen. The refined products can be used for the same purposes as those derived from crude oil. The term "shale oil" is also used for crude oil produced from shales of other unconventional, very low permeability formations. However, to reduce the risk of confusion of shale oil produced from oil shale with crude oil in oil-bearing shales, the term " tight oil" is preferred for the latter. The International Energy Agency recommends to use the term " light tight oil" and World Energy Resources 2013 report by the World Energy Council uses the term " tight oil" for crude oil in ...
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Oil Shale Gas
Oil shale gas (also: retort gas or retorting gas) is a synthetic non-condensable gas mixture (syngas) produced by oil shale thermal processing (pyrolysis). Although often referred to as shale gas, it differs from the natural gas produced from shale, which is also known as shale gas. Process Oil shale gas is produced by retorting (pyrolysis) of oil shale. In the pyrolysis process, oil shale is heated until its kerogen decomposes into vapors of a petroleum-like condensable shale oil, non-condensible combustible oil shale gas, and spent shale—a solid residue. The process is the same as the shale oil extraction and oil shale gas usually occurs as a byproduct of shale oil production. The ratio of oil shale gas to shale oil depends on retorting temperature and as a rule, increases by the rise of temperature. Composition There is no exact formula of oil shale gas. Compositions of oil shale gas depends on the retorted oil shale and exploited technology. Typical components o ...
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Condenser (laboratory)
In chemistry, a condenser is laboratory apparatus used to condense vaporsthat is, turn them into liquidsby cooling them down. Condensers are routinely used in laboratory operations such as distillation, reflux, and extraction. In distillation, a mixture is heated until the more volatile components boil off, the vapors are condensed, and collected in a separate container. In reflux, a reaction involving volatile liquids is carried out at their boiling point, to speed it up; and the vapors that inevitably come off are condensed and returned to the reaction vessel. In Soxhlet extraction, a hot solvent is infused onto some powdered material, such as ground seeds, to leach out some poorly soluble component; the solvent is then automatically distilled out of the resulting solution, condensed, and infused again. Many different types of condensers have been developed for different applications and processing volumes. The simplest and oldest condenser is just a long tube through ...
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Charcoal
Charcoal is a lightweight black carbon residue produced by strongly heating wood (or other animal and plant materials) in minimal oxygen to remove all water and volatile constituents. In the traditional version of this pyrolysis process, called charcoal burning, often by forming a charcoal kiln, the heat is supplied by burning part of the starting material itself, with a limited supply of oxygen. The material can also be heated in a closed retort. Modern "charcoal" briquettes used for outdoor cooking may contain many other additives, e.g. coal. This process happens naturally when combustion is incomplete, and is sometimes used in radiocarbon dating. It also happens inadvertently while burning wood, as in a fireplace or wood stove. The visible flame in these is due to combustion of the volatile gases exuded as the wood turns into charcoal. The soot and smoke commonly given off by wood fires result from incomplete combustion of those volatiles. Charcoal burns at a highe ...
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Alembic
An alembic (from ar, الإنبيق, al-inbīq, originating from grc, ἄμβιξ, ambix, 'cup, beaker') is an alchemical still consisting of two vessels connected by a tube, used for distillation of liquids. Description The complete distilling apparatus consists of three parts: the "cucurbit" (Arabic: ; Greek: , ), the still pot containing the liquid to be distilled, which is heated by a flame; the "head" or "cap" (, ; Greek , ) which fits over the mouth of the cucurbit to receive the vapors, with an attached downward-sloping "tube" (, ); and the "receiver" (, ; , or , ) container. In the case of another distilling vessel, the retort, the "cap" and the "cucurbit" have been combined to form a single vessel. The anbik is also called the raʾs (head) of the cucurbit. The liquid in the cucurbit is heated or boiled; the vapour rises into the anbik, where it cools by contact with the walls and condenses, running down the spout into the receiver. A modern descendant of the al ...
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Phosphorus
Phosphorus is a chemical element with the symbol P and atomic number 15. Elemental phosphorus exists in two major forms, white phosphorus and red phosphorus, but because it is highly reactive, phosphorus is never found as a free element on Earth. It has a concentration in the Earth's crust of about one gram per kilogram (compare copper at about 0.06 grams). In minerals, phosphorus generally occurs as phosphate. Elemental phosphorus was first isolated as white phosphorus in 1669. White phosphorus emits a faint glow when exposed to oxygen – hence the name, taken from Greek mythology, meaning 'light-bearer' (Latin ), referring to the "Morning Star", the planet Venus. The term '' phosphorescence'', meaning glow after illumination, derives from this property of phosphorus, although the word has since been used for a different physical process that produces a glow. The glow of phosphorus is caused by oxidation of the white (but not red) phosphorus — a process now called che ...
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